2004 Winter Conference on
Plasma
Spectrochemistry
Fort Lauderdale, Florida, January 5-10, 2004
Winter Conference ICP Information Newsletter URIAC
Final Program
2004 Winter Conference on Plasma Spectrochemistry
Fort Lauderdale, Florida, January 5-10, 2004
Monday, January 5, 2004
1. Sample Introduction and Transport Phenomena
Akbar Montaser, Chair
08:00 Opening and Welcome. Ramon M. Barnes
08:05 PL01 Comparing Atomic Spectrometric Methods to the "Super Stars": Special Emphasis on LIBS, A Future Super Star? James D. Winefordner, University of Florida, Department of Chemistry, P.O. Box 117200, Gainesville FL 32611-7200, jdwin@chem.ufl.edu; Tiffany Correll, Emily Gibb, Igor Gornushkin, Nicolo Omenetto, and Benjamin Smith
09:00 IL01 Sample Introduction and Sample Plasma Interactions. John W. Olesik, Ohio State University, Department of Geological Sciences, 125 S. Oval Mall, 275 Mendenhall, Columbus OH 43210, olesik.2@osu.edu
09:30 IL02 Fundamental Nebulization Processes and Analyte Transport. Akbar Montaser, The George Washington University, Department of Chemistry, 725 21st St., NW, Washington DC 20052, montaser@gwu.edu
10:00 Break (Sponsored by Bristol-Myers Squibb Company)
10:20 M01 Plasma Spectrochemical Analysis of Petroleum Naphthas Using Low Flow Sample Introduction Equipment. Robert I. Botto, ExxonMobil Chemical Company, Baytown Chemical Plant Laboratory, 4500 Bayway Drive, Baytown TX 77520, bob.i.botto@exxonmobil.com
10:40 M02 Taming the Free Up-Take of Pneumatic Nebulizers. Nimal De Silva, Carleton University, Department of Chemistry, Ottawa ON K1S 5B2, Canada, ndesilva@ccs.carleton.ca
11:00 M03 Routine CE ICP/MS Speciation Analysis with the Mira Mist CE Interface -- Problems and Advantages. John A. Burgener, Burgener Research Inc., 1680-2 Lakeshore Road W., Mississauga ON L5J 1J5, Canada, burgener@burgenerresearch.com; Eric Hoffman, Yakov Kapusta, and M. Dzierzgowska
11:20 M04 Transport Efficiencies and Their Impact on Precision and Sensitivity for ETV Sample Introduction into ICPMS. James A. Holcombe, University of Texas at Austin, Department of Chemistry and Biochemistry, 1 University Station A5300, Austin TX 78712-0165, holcombe@mail.utexas.edu; Gulay Ertas, Nikhilesh Desai
11:40 M05 Nano Particle Sample Introduction (PSI) System for Inductively Coupled Plasma - Atomic Emission Spectrometry (ICP-AES). Vassili Karanassios, University of Waterloo, Department of Chemistry, Waterloo ON N2L 3G1, Canada, vkaranassios@uwaterloo.ca; Lowell Greib
12:00 Lunch Break
Monday, January 5, 2004
2. Elemental Speciation: Sampling and Preparation
Les Ebdon, Chair
1:00 IL03 SPME for Organometallic Speciation Measurement - Sample Preparation Made Easy. Ralph Sturgeon, Institute for National Measurement Standards, National Research Council of Canada, Montreal Road, Bldg M-12, Ottawa ON K1A 0R9, Canada, ralph.sturgeon@nrc.ca; Zoltan Mester, Lu Yang, Patricia Grinberg, and Scott Willie
1:30 IL04 Sample Preparation for Elemental Speciation. Olivier F.X. Donard, Université de Pau, Laboratoire de Chimie Analytique Bioinorgnique et Environnement, CNRS UMR 5034, Hélioparc, 2 Avenue du Président Angot, F-64053 Pau, France, olivier.donard@univ-pau.fr
2:00 M06 "New" Adventures with "Old" Chelating Agents. Gas Chromatography of Metal Chelates Using Modern Extraction and Detection Methods. Zoltan Mester, National Research Council of Canada, Institute for National Measurement Standards, 1500 Montreal Road, Ottawa ON K1A 0R6, Canada, zoltan.mester@nrc.ca
2:20 M07 Use of Accelerated Solvent Extraction for Organotin Speciation in Biological Matrices. Roberto Morabito, ENEA-PROT, Via Anguillarese, 301, I-0060 Rome, Italy, morabito@casaccia.enea.it; Paolo Massanisso
2:40 M08 Application of a Triple Spike Methodology for the Determination of Butyltin Compounds in Biological Materials by Isotope Dilution Mass Spectrometry. Pablo Rodríguez-González, University of Oviedo, Department of Physical and Analytical Chemistry, Julian Caveria 8, E-33006 Oviedo, Spain, pablorodg@yahoo.com; J. Igancio García Alonso, and Alredo Sanz-Medel
3:00 Break (Sponsored by Bristol-Meyers Squibb Company)
3:20 M09 Application of Ion Chromatography (IC) with Inductively Coupled Plasma Mass Spectrometric (ICP-MS) Detection for the Characterization of Waste Materials. Jeffrey Giglio, Argonne National Laboratory - West, P.O. Box 2528, Idaho Falls ID 83404, jeff.giglio@anlw.anl.gov; Cal Morgan, Marianne Noy, and Daniel Cummings
3:40 M10 Analysis of Uranium/Plutonium Materials with Micro-Column Extraction with Inductively Coupled Plasma Mass Spectrometric (ICP-MS) Detection. Marianne Noy, Argonne National Laboratory - West, P.O. Box 2528, Idaho Falls ID 83404, jeff.giglio@anlw.anl.gov; Daniel Cummings, and Jeffrey Giglo
4:00 M11 Mercury Speciation in Aquatic Biota by HPLC/ICP-OES. Mary Kate Donais, Saint Anselm College, Department of Chemistry, 100 Saint Anselm Drive #1705, Manchester NH 03102-1310, mdonais@anselm.edu; David L. Pfeil
4:20 M12A FI-CE-ICP-MS System with On-Line Preconcentration for Determination of Inorganic Selenium Species. Carlos E.S. Miranda, Universidade de Săo Paulo, Instituto de Química de Săo Carlos, P.O. 780, 13566-590, Săo Carlos, SP, Brazil, mfgine@cen.sp.br; Emanuel Carrilho, Ana Paula G. Gervasio, Ana Claudia S. Bellato, and Maria Fernanda Giné
4:40 M13 Speciation Using Hyphenation of Microseparation Techniques with ICP-MS. Nancy J. Miller-Ihli, US Department of Agriculture, Food Composition Laboratory, Rm 1, Bldg. 161 BARC-East, Beltsville MD 20705, miller-ihli@bhnrc.usda.gov; Enrique G. Yanes
5:00 M14 Ion Pair Chromatography Coupled to ICP-HR-MS for the Determination of Phytate and Its Metabolites. Jörg Bettmer, Johannes Gutenberg-University Mainz, Institute of Inorganic Chemistry and Analytical Chemistry, Duesbergweg 10-14, D-55099 Mainz, Germany, bettmer@mail.uni-mainz.de; Andreas Helfrich
Panel Discussion
5:30 PD01 Sample Introduction. Jean-Michel Mermet, Unversité Claude Bernard - Lyon I, Laboratoire des Sciences Analytiques, Batiment 308, F-69622 Villeurbanne Cedex, France, mermet@cpe.fr; John Olesik, Akbar Montaser, Robert I. Botto, and Nimal De Silva
6:30 Exhibition Opening and Social Mixer
Tuesday, January 6, 2004
3. Elemental Speciation
Peter C. Uden, Chair
08:00 PL02 Elemental Speciation: Present Problems and Future Prospects. Freddy C. Adams, University of Antwerp (UIA), Micro and Trace Analysis Centre, Universiteitsplein 1, B-2610 Wilrijk, Belgium, adams@uia.ua.ac.be
09:00 IL05 Element Speciation in Biological Materials by ICP-MS: A Road to the Proteomics World. Alfredo Sanz-Medel, University of Oviedo, Department of Physical and Analytical Chemistry, c/ Julián Clavería, 8, E-33006 Oviedo, Spain, asm@correro.uniovi.es
09:30 IL06 Inductively Coupled Plasma Mass Spectrometry in Proteomics Research. Ryszard Lobinski, Group of Bio-Inorganic Analytical Chemistry, CNRS UMR 5034, Hélioparc, 2 av. du Pr. Angot, F-94053 Pau, France, ryszard.lobinski@univ-pau.fr
10:00 Break (Sponsored by Agilent Technologies)
10:20 T01 Speciation of Arsenic, Selenium and Chromium in Leachates and Pore Waterwaters at Coal-Combustion By-Product Storage Facilities. Dirk Wallschläger, Trent University, Environmental & Resource Studies Program, 1600 West Bank Dr, Peterborough ON K9J 7B8, Canada, dwallsch@trentu.ca; Claudio N. Ferrarello
10:40 T02 Are Chicken Farms the Newest Source of Arsenic Contamination? Hakan Gürleyük, Frontier Geosciences, Inc., 414 Pontius Ave. N., Suite B, Seattle WA 98109-5461, hakang@frontiergeosciences.com; Jeni Garcia, Bob Brunette, and Rod O’Connor
11:00 T03 Determination of Arsenosugars with HPLC-HG-ICPMS. Ernst Schmeisser, Karl-Franzenzs-University of Graz, Institute of Chemistry - Analytical Chemistry, Universtitätsplatz 1, A-8010 Graz, Austria, ernst.schmeisser@uni-graz.at; Walter Goessler, and Kevin A. Francesconi
11:20 T04 Characterization of Novel Selenium Volatiles Utilizing GC-ICP-MS/GC-TOF-MS and Quantum Chemistry Modeling Techniques. Juris Meija, University of Cincinnati, Department of Chemistry, P.O. Box 0172, Cincinnati OH 45221, meijaj@email.uc.edu; Thomas L. Beck, and Joseph A. Caruso
11:40 T05 Selenium Conjugates with Biological Thiols as Mean of Entering Se Metabolic Pathway in Biological Samples. Maria Montes Bayón, University of Oviedo, Department of Physical and Analytical Chemistry, c/Julián Clavería 8, E-33006 Oviedo, Spain, montesm@email.uc.edu; Paula Braga Riera, Jesús Alvarez-Pińera, and Alfredo Sanz-Medel
12:00 Lunch Break
Tuesday, January 6, 2004
4. Elemental Speciation
Joseph A. Caruso, Chair
1:00 IL07 In Search of Accuracy in Elemental Speciation Analysis. Rita Cornelis, University of Ghent, Laboratory for Analytical Chemistry, Proeftuinstraat 86, B-9000 Gent, Belgium, rita.cornelis@ugent.be
1:30 T06 Atomic and Molecular Mass Spectrometry for Characterizing Selenium Containing Proteins in Brassica Juncea. Sandra Mounicou, University of Cincinnati, Department of Chemistry, Box 0172, Cincinnati OH 45223-0172, mounicsn@email.uc.edu; Juris Meija, Baki B.M. Sadi, Patrick A. Limbach, and Joseph A. Caruso
1:50 T07 Natural Iron Isotopic Variation in Whole Blood, Serum and Serum Proteins in Individuals with HFE Mutations. Christian Wolf, Institute of Food Research, Norwich Research Park, Colney, Norwich NR4 7UA, United Kingdom, christian.wolf@bbsrc.ac.uk; Jurian Hoogewerff, Mark Roe, Jack Dainty, Birgit Teucher, and Sue Fairweather-Tait
2:10 T08 Analysis of Phosphorus Herbicides by Ion-Pairing Reversed Phase HPLC Coupled to ICP-MS Detection with Collision Cell. Baki B.M. Sadi, University of Cincinnati, Department of Chemistry, Analytical Division, Mail Box 0172, Cincinnati OH 45221-0172, sadibm@email.uc.edu; Ann P. Vonderheide and Joseph A. Caruso
2:30 T09 Comprehensive Organic/Inorganic Arsenic Speciation and Detection Using Particle Beam Glow Discharge Mass Spectrometry. Jake L. Venzie, Clemson University, Department of Chemistry, 102 BRC Laboratory, Clemson SC 29634-0973, jvenzie@clemson.edu; W. Clay Davis, and R. Kenneth Marcus
2:50 T10 Gas Chromatography Combined with Fast Flow Glow Discharge Mass Spectrometry. Karla Newman, University of Wales Swansea, Department of Chemistry, Singleton Park, Swansea SA2 8PP, United Kingdom, karla_newman@isic.org; Rod S. Mason
3:00 – 6:30 Poster Session: Sample Introduction, Sampling and Sample Preparation, Element Speciation
Poster Session: Sample Introduction
TP01 Design and Evaluation of a New Direct Injection Argon/Helium ICP Torch. Akitoshi Okino, Tokyo Institute of Technology, Department of Energy Sciences, 4259 Nagatsuta, Midori-ku, Yokohama 226-8502, Japan, aokino@es.titech.ac.jp; Hidekazu Miyahara, Hironobu Yabuta, Yoicho Mizusawa, Takayuki Doi, Masato Watanabe, and Eiki Hotta
TP02 Characterization of a Tungsten-ETV Device with Regards to Sample Introduction into Analytical Plasma Sources. Nicolas H. Bings, University of Hamburg, Institute for Inorganic and Applied Chemistry, Martin-Luther-King Platz 6, D-20146 Hamburg, Germany, bings@chemie.uni-hamburg.de; Volker Siemens
TP03 Transport Efficiencies and Their Impact on Precision and Sensitivity for ETV Sample Introduction into ICPMS. Nikhilesh Desai, University of Texas at Austin, Department of Chemistry and Biochemistry, 1 University Station A5300, Austin TX 78712-0165, nikhilesh@mail.utexas.edu; James A. Holcombe
TP04 Evaluating Robustness of an Ar-N2 Mixed Gas Plasma for ETV-ICPMS. William J. Balsanek, University of Texas at Austin, Department of Chemistry and Biochemistry, 1 University Station A5300, Austin TX 78712-0165, balsanek@yahoo.com; James A. Holcombe
TP05 Determination of Metallic Impurities in Al2O3 by ETV-ICP-MS Using Thermochemical Modifiers. José A.C. Broekaert, University of Hamburg, Department of Chemistry, Martin-Luther-King-Platz 6, D-20146 Hamburg, Germany, jose.broekaert@chemie.uni-hamburg.de; Birgit Peschel, Nicolas H. Bings
TP06 Application of a Novel Sample Introduction System for VPD ICP-MS. David Bollinger, Air Liquide - Balazs Analytical Service, 13546 N. Central Expressway, MS 3, Dallas TX 75243, david.bollinger@airliquide.com; Scott Anderson
TP07 Evaluation of Parallel Path Nebulizer for ICP-MS Analysis of Various Matrices Compared with Cross Flow Nebulizer. Ying Zhou, GE Global Research, One Research Circle, Bldg K-1, Room 2A30, Niskayuna NY 12309, zhouy@crd.ge.com; Antoaneta Krushevska
TP08 Analysis of Volatile Organic Solvents by Sector Field ICP-MS. Julian D. Wills, Thermo Electron, 2 Barkhausenstrasse, D-28197 Bremen, Germany, julian.wills@thermo.com
TP09 Some Biological and Clinical Applications of In-Torch Vaporization Inductively Coupled Plasma Spectrometry (ITV-ICP). Vassili Karanassios, University of Waterloo, Department of Chemistry, Waterloo ON N2L 3G1, Canada, vkaranassios@uwaterloo.ca; Hamid Badiei, Blair Gibson, Bithi Eshque, Darryl Ward, and Andrea Smith
TP10 Electrostatic Particle Sampler (EPS) for Collection of Airborne Particles and Subsequent Analysis by In-Torch Vaporization Inductively Coupled Plasma (ITV-ICP) Spectrometry. Vassili Karanassios, University of Waterloo, Department of Chemistry, Waterloo ON N2L 3G1, Canada, vkaranassios@uwaterloo.ca; Greg Sprah
TP11 Analysis of High-Purity Gold by Axial View ICP-AES with Spark Ablation and Ultrasonic Nebulization. George Glavin, Spectro Analytical Instruments, Inc., 160 Authority Dr., Fitchburg MA 01420, ggglavin@spectro-usa.com; Sergei Leikin
TP12 A Simple Hydride Generation CE-ICP-MS Interface for Arsenic Speciation. Douglas D. Richardson, University of Cincinnati, Department of Chemistry, Mail Location 0172, Cincinnati OH 45221-0172, richard2@email.uc.edu; Rodolfo G. Wuilloud, Sasi S. Kannamkumarath, and Joseph A. Caruso
TP13 Recent Developments in Direct Powder Introduction -- Inductively Coupled Plasma (DPI-ICP) Spectrometry. Nimal De Silva, Carleton University, Department of Chemistry, Ottawa ON K1S 5B2, Canada, ndesilva@ccs.carleton.ca; Isa Mohammed, Davide Bleiner, and Conrad Gregoire
TP14 Sedimented Slurry Nebulization - Inductively Coupled Plasma Spectrometry (SSN-ICP). Nimal De Silva, Carleton University, Department of Chemistry, Ottawa ON K1S 5B2, Canada, ndesilva@ccs.carleton.ca; Isa Mohammed, Ibraheem Gaabass
Poster Session: Sampling and Sample Preparation
TP15 Preparation of Stable Slurry for Sample Introduction in Analytical Atomic Spectrometry. Zheng Wang, Shanghai Institute of Ceramics, Chinese Academy of Sciences, 1295 Dingxi Road, Shanghai 200050, China, wangzheng_sh@163.com; Zheming Ni, Deren Qiu, Tianyu Chen, Guagyi Tao, Pengyuan Yang
TP16 Elemental Fractionation and Quantification of Natural Water Colloids by FlFFF-HR ICP MS: Development and Validation of a Method. Karen Andersson, Göteborg University, Analytical and Marine Chemistry, Kemivägen 10, SE-412 96 Göteborg, Sweden, bjorn@amc.gu.se; Björn Stolpe, Tobia Larsson, and David Turner
TP17 Determination of Trace Metal Distribution in Humic and Fulvic Acids by Capillary Electrophoresis - Inductively Coupled Plasma Mass Spectrometry (CE-ICPMS). John C. Danku, University of Massachusetts, Department of Chemistry, 701 LGRCT, 710 N. Pleasant St., Amherst MA 01003-9336, danku@chem.umass.edu; Ramon M. Barnes, and Dula Amarasiriwardena
TP18 Determination of REE at Ultratrace Levels by On-Line Preconcentration Coupled to Anion Exchange Chromatography - ICP-MS. Jose Ignacio García Alonso, University of Oviedo, Department of Physical and Analytical Chemistry, Julian Caveria 8, E-33006 Oviedo, Spain, ngalonso@correo.uniovi.es; Ruben Garcia-Fernández, and Alredo Sanz-Medel
TP19 Preconcentration and Determination of Traces of Antimony in Environmental and Pharmaceutical Samples. Alexandra Lásztity, Eötvös L. University, Department of Inorganic and Analytical Chemistry, P.O. Box 32, H-1518 Budapest, Hungary, lasztity@para.chem.elte.hu; Katalin Zih-Perényi, Imre Varga, and Éva Sugár
TP20 Speciation of Essential and Toxic Elements in Edible Mushrooms by SEC-UV-ICP-MS. Rodolfo G. Wuilloud, University of Cincinnati, Department of Chemistry, Mail Location 0172, Cincinnati OH 45223-0172, joseph.caruso@uc.edu; Sasi S. Kannmkumarath, and Joseph A. Caruso
TP21 Speciation Analysis of Organotin Compounds. Investigations on the Derivatisation Using a Non-Focussed Microwave System. Herbert Fruhmann, Graz University of Technology, Institute for Analytical Chemistry, Micro- and Radiochemistry, Technikerstrasse 4, A-8010 Graz, Austria, fruhmann@analytchem.tugaz.at; Günter Knapp, and Michael Zischka
TP22 Simultaneous Extraction of Organometallic Species of As, Sn, and Hg by Accelerated Solvent Extraction and Analysis by ICP-MS Coupled to Liquid- and Gas-Chromatography. Raimund Wahlen, LGC Limited, Queen's Road, Teddington Middlesex TW11 OLY, United Kingdom, raimund.wahlen@lgc.co.uk; Mark Scrimshaw, Paul Norris, and Tim Catterick
Poster Session: Elemental Speciation Analysis
TP23 Total and Speciated Arsenic Measurements in Commercially Available Peanut Butter Spread by ICPMS and IC/HG/ICPMS. B. Michael Hovanec, West Coast Analytical Service, 9240 Santa Fe Springs Road, Santa Fe Springs CA 90670, mike.hovanec@wcaslab.com
TP24 Challenges Associated with the Determination of Non-Dietary Arsenic in Urine by Inductively Coupled Plasma Mass Spectrometry (ICP-MS). Ela Bakowska, National Medical Services, 3701 Welsh Road, Willow Grove PA 19090, ela.bakowska@nmslab.com; Maoch Muantongchin, and Judy Vinosky
TP25 Investigation of "Hidden" Arsenicals at Ultra-trace Levels in Biological Samples by LC-Hydride Generation - ICPMS Combined with a High-Efficiency Photoxidation Reactor. Tetsuya Nakazato, National Institute of Advanced Industrial, Science and Technology (AIST), 16-1 Onogawa, Tsukuba-shi, Ibaraki 305-8569, Japan, tet.nakazato@aist.go.jp; Hiroaki Tao
TP26 Arsenic Speciation in Urine by DRC-ICP-MS: Validation and Characterization, the CDC Experience. Carl P. Verdon, Centers for Disease Control and Prevention, 4770 Buford Hwy NE, Mail Stop F-18, Atlanta GA 30341-3724, cverdon@cdc.gov; Kathy L. Caldwell, Robert L. Jones, and Mark Fresquez
TP27 The Determination of Total and Speciated Arsenic in Samples of Potatoes, Yams and Wheat Using ICP-MS. Kevin Kubachka, University of Cincinnati, Department of Chemistry, Mail Location 0172, Cincinnati OH 45221-0172, kubachk@email.uc.edu; Pamela R. Halpin, Douglas T. Heitkemper, and Joseph A. Caruso
TP28 HPLC-ICP-MS Speciation of Arsenic in Different Types of Nuts. Sasi Kannamkumarath, University of Cincinnati, Department of Chemistry, Mail Location 0172, Cincinnati OH 45223-0172, kannamss@email.uc.edu; Kazimierz Wróbel, Katarzyna Wróbel, and Joseph A. Caruso
TP29 Determination of Arsenic Containing Compounds in Poultry Samples Using IC-ICP-MS. Tyre D. Grant, U.S. Food and Drug Administration, 6751 Steger Dr., Cincinnati OH 45237, tgrant2@ora.fda.gov; Douglas T. Heitkemper, and Joseph A. Caruso
TP30 Determination of Arsenical Species in Water Sources, Urine and Hair from Exposed Population in Atacama, Chile. Jorge Yańez S., University of Concepción, Faculty of Chemistry, Department of Analytical and Inorganic Chemistry, Edmundo Larenas 129, Concepción, Chile, jyanez@udec.cl; V. Fierro, H.D. Mansilla, L. Figueroa, L. Cornejo, and R.M. Barnes
TP31 The Analytical Potential of Capillary Electrophoresis for the Quantification of As Species. Sergio Caroli, Istituto Superiore di Sanitŕ, Viale Regina Elena 299, I-00161 Rome, Italy, caroli@iss.it; M. D'Amato, and G. Forte
TP32 As Speciation by ICP-MS: Effect of the Nebulization System on the Response for the Various As Species. Fadi Abou-Shakra, GV Instruments, Crews Road, Wythenshawe, Manchester M23 9BE, United Kingdom, fadi.aboushakra@gvinstruments.co.uk; Steve Shuttleworth
TP33 Evaluation of Genetic Modifications to Improve Phytoremediation of As, Cd, and Se in Brassica Juncea Plants by Mass Spectrometric Techniques. Maria Montes-Bayón, University of Oviedo, Department of Physical and Analytical Chemistry, c/Julian Claveria 8, E-33006 Oviedo, Spain, montesm@email.uc.edu; Juris Meija, Joseph A. Caruso, and Alfredo Sanz-Medel
TP34 Identification and Characterization of Selenium Species in Enriched Green Onion (Allium fistulosum) by HPLC-ICP-MS and ESI-ITMS. Monika Shah, University of Cincinnati, Department of Chemistry, Mail Location 0172, Cincinnati OH 45223-0172, joseph.caruso@uc.edu; Sasi S. Kannmkumrath, Jorgelina C.A. Wuilloud, Rodolfo G. Wuilloud, and Joseph A. Caruso
TP35 Identification and Characterization of Selenoproteins in Selenium Enriched Saccharomyces Uvaum. Katie DeNicola, University of Cincinnati, Department of Chemistry, Mail Location 0172, Cincinnati OH 45221, k_denicola@hotmail.com; Sandra Mounicou and Joseph A. Caruso
TP36 Simultaneous Monitoring of Selenium and Sulfur in Volatile Species from Selenium Enriched Samples by GC-AED and GC-MS. Harriet Totoe Boakye, University of Massachusetts, Department of Chemistry, 701 Lederle GRC Tower, Amherst MA 01003-9336, pcuden@chem.umass.edu; Julian F. Tyson, Peter C. Uden, and Eric Block
TP37 Application of Sector-Field ICP-MS for Metallothionein Study in Human Thyroids with Account of Environmental Peculiarities. Sergei F. Boulyga, Johannes Gutenberg-University Mainz, Institute of Inorganic Chemistry and Analytical, Duesbergweg 10-14, D-55099 Mainz, Germany, boulyga@uni-mainz.de; Valeria Loreti, Jörg Bettmer
TP38 Comparative Speciation Study of Cancer and Healthy Thyroids. Sergei F. Boulyga, Johannes Gutenberg-University Mainz, Institute of Inorganic Chemistry and Analytical, Duesbergweg 10-14, D-55099 Mainz, Germany, boulyga@uni-mainz.de; Valeria Loreti, Jörg Bettmer, Klaus G. Heumann
TP39 Nickel Species Analysis of Nickel Incubated HT29/B6 Cell Line Using Multidimensional HPLC and SF-ICP-MS. Tina Knispel, GKSS-Research Center, Institute of Coastal Research/Physical and Chemical Analysis, Max-Planck Straße 1, D-21502 Geesthacht, Germany, tina.knispel@gkss.de; M. Kühbacher, Evelin Denkhus, Andreas Prange, A. Kyriakopoulos, and D. Behne
TP40 Multielement Distribution Pattern of Premature Human and Pre-Term Milk Whey by SEC-ICP- (ORC) MS. Alfredo Sanz-Medel, University of Oviedo, Department of Physical and Analytical Chemistry, c/ Julian Clavería, 8, E-33006 Oviedo, Spain, asm@sauron.quimica.uniovi.es; Rafel R. de la Flor St. Remy, Maria Luisa Fernández Sanchez, and José López Sastre
TP41 HPLC Coupled to Sector-Field ICP-MS and Hybrid Ion Trap Fourier Transform Mass Spectrometry as Complementary Techniques for Pharmaceutical Applications. Torsten Lindemann, Thermo Electron, Barkhausenstrasse 2, D-28197 Bremen, Germany, torsten.lindemann@thermo.com
TP42 Analysis of Cisplatin and Its Hydrated Complexes by ESI-MS and High-Field Asymmetric Waveform Ion Mobility Spectrometry. Meng Cui, National Research Council of Canada, Institute for National Measurement Standards, 1200 Montreal Road M12, G7, Ottawa ON K1A 0R6, Canada, zoltan.mester@nrc.ca; Luyi Ding, and Zoltan Mester
TP43 Characterization of the Liquid Sampling - Atmospheric Pressure Glow Discharge Plasma for Microbore HPLC Detection. Jake Venzie, Clemson University, Department of Chemistry, 102 BRC Laboratory, Clemson SC 29634-0973, jvenzie@clemson.edu; R. Kenneth Marcus
TP44 Effects of Easily Ionizable Elements (EIES) in the Liquid Sampling Atmospheric Glow Discharge Plasma. Jake Venzie, Clemson University, Department of Chemistry, 102 BRC Laboratory, Clemson SC 29634-0973, jvenzie@clemson.edu; W. Clay Davis, and R. Kenneth Marcus
TP45 Quantification and Characterization of Sulfur in Low Sulfur Reformulated Gasolines by GC/ICP-MS. Steve M. Wilbur, Agilent Technologies, 3380 146th Pl SE, Suite 300, Bellevue WA 98007-6472, steven_wilbur@agilent.com; Ed McCurdy
TP46 The Potential of ICP-MS as an Element Specific Detector for Capillary Electrophoresis Separation of Pesticides. Rodolfo G. Wuilloud, University of Cincinnati, Department of Chemistry, Mail Location 0172, Cincinnati OH 45223-0172, joseph.caruso@uc.edu; Monika Shah, Sasi S. Kannamkumarath, and Joseph A. Caruso
TP47 Fission Products Determination by CE-EIS-MS and Comparison with IC-ICP-MS. Aurlélien Pitois, Institute for Tansuranium Elements, Joint Research Centre - European Commission, P.O. Box 2340, D-76125 Karlsruhe, Germany, aurelien.pitois@itu.fzk.de; Maria Betti, and Laura Aldave de las Heras
TP48 Fast Separation and Determination of Iodophenol Species in Natural Waters by Solid-Phase Microextraction with CE-ICP-MS Detection. Sasi Kannamkumarath, University of Cincinnati, Department of Chemistry, Mail Location 0172, Cincinnati OH 45223-0172, kannamss@email.uc.edu; Rodolfo G. Wuilloud, Sarath Jayasinghe, and Joseph A. Caruso
TP49 Determination of Halogen Speciation in Waters by Ion Chromatography - Inductively Coupled Plasma - Mass Spectrometry -- Is It Possible? Dirk Wallschläger, Trent University, Environmental & Resource Studies Program, 1600 West Bank Dr, Peterborough ON K9J 7B8, Canada, dwallsch@trentu.ca; Hakan Gürleyük
TP50 Determination of Bobel-24 Anti-Inflammatory and Its Metabolites in Human Urine by HPLC-ICP-MS. Rodolfo G. Wuilloud, University of Cincinnati, Department of Chemistry, Mail Location 0172, Cincinnati OH 45223-0172, joseph.caruso@uc.edu; Niranjan Selar, Sasi S. Kannamkumarath, and Joseph A. Caruso
TP51 Direct and Indirect Speciation Analysis of Metal Ions in Waters and Soil Extracts. Hakan Gürleyük, Frontier Geosciences, Inc., 414 Pontius Ave. N., Suite B, Seattle WA 98109-5461, hakang@frontiergeosciences.com
TP52 Determination of Trace Amounts of Phosphorus and Phosphates in Waters. Hakan Gürleyük, Frontier Geosciences, Inc., 414 Pontius Ave. N., Suite B, Seattle WA 98109-5461, hakang@frontiergeosciences.com; Jeni Garcia
TP53 The Liaison of Organic and Inorganic Chemistry: Determination of Heteroelements for the Elemental Speciation of Pesticides in Environmental Samples by GC-Collision-Cell-ICP-MS. Daniel Proefrock, GKSS-Research Center, Institute for Coastal Research, Max-Planck Straße 1, D-21502 Geesthacht, Germany, daniel.proefrock@gkss.de; P. Leonard, A. Prange, and Steven Wilbur
TP54 Development of Hyphenated Systems for a Bio-Response Linked Instrumental Analysis (BLIA) Based on Element- and Molecule Specific Detection Techniques and Their Application on the Determination of DNA Nucleotides and DNA Adducts. Daniel Proefrock, GKSS-Research Center, Institute for Coastal Research, Max-Planck Straße 1, D-21502 Geesthacht, Germany, daniel.proefrock@gkss.de; Angreas Prange
TP55 Quantification of Methylmercury and Inorganic Mercury in Shark Filets - Results of Different Techniques As Well As Influence of Sample Handling on Fresh Fish Material. Petra Krystek, National Institute of Public Health and Environment RIVM, Laboratory of Analytical Chemistry, P.O. Box 1, NL-3720 BA Bilthoven, The Netherlands, petra.krystek@rivm.nl; Rob Ritsema
TP56 Optimization of HPLC and ICP-MS for Iron Speciation in the Environment. Alison E. Holliday, Laboratoire de Chimie Analytique Bio-inorganique, CNRS UMR 5034, Helioparc, 2 av. Pierre Angot, F-64000 Pau, France, alison.holliday@etud.univ-pau.fr; Eva Krupp, Mariella Moldovan, Christophe Pécheyran, O.F.X. Donard, and Diane Beauchemin
TP57 Determination and Speciation of Chromium by Laser Induced Breakdown Spectroscopy. Scott R. Goode, University of South Carolina, Department of Chemistry and Biochemistry, Columbia SC 29208, goode@sc.edu; Christopher R. Dockery, and Jack E. Pender
TP58 Application of Atomic Spectrometric Methods Coupled with Gas Chromatography for Geochemical Exploration. Galina Mazo, Lomonosov Moscow State University, Department of Chemistry, Leninskie Gory, Moscow 119899, GSP-2, Russia, mazo@inorg.chem.msu.ru; N.S. Safronova
Workshop on New Plasma Instrumentation, Sample Preparation, and Accessories
Isaac (Joe) Brenner and Robert I. Botto, Chairs
Introduction
3:15 WS100 Setting the Scene - Challenges of Inductively Coupled Plasma Atomic and Mass Spectrometry. Isaac (Joe) Brenner, Environmental Analytical Services, 9 Dishon Street, Apartment 9, Malkha, Jerusalem 96956, Israel, brenner@cc.huji.ac.il
3:30 WS101 Setting the Scene - Plasma Instrumentation and Sample Preparation: A Practical Viewpoint. Robert I. Botto, ExxonMobil Chemical Company, Baytown Chemical Plant Laboratory, 4500 Bayway Drive, Baytown TX 77520, bob.i.botto@exxonmobil.com
Sample Introduction
3:50 WS102 New Developments in Burgener Nebulizers. John Burgener, Burgener Research Inc., 1680-2 Lakeshore Road W., Mississauga ON L5J 1J5, Canada, burgener@burgenerresearch.com
4:10 WS103 A Focus on Recent Developments in Sample Introduction for ICP-AES and MS. Jerry Dulude, Glass Expansion, Inc., 4 Barlows Landing, Suite 2, Pocasset, MA 02559-1983, jdulude@adelphia.net
Inductively Coupled Plasma –Atomic Emission Spectroscopy
4:30 WS104 New ICP-AES and RF-GD-OES Instrument Developments and Applications in Jobin Yvon. Geoff Tyler, Jobin Yvon SA, 16-18, rue du Canal, F-91165 Longjumeau Cedex, France, geoftyler@aol.com; Agnčs Cosnier, Nathalie Le Corre, Sébstien Velasquez, and Patrick Chapon
4:50 WS105 Achieving Exceptional Analytical Performance in ICP-OES: A New Spectrometer with a Large Format Programmable Array Detector. Peter G. Brown, Leeman Labs, Inc., 6 Wentworth Dr., Hudson NH 03051, pbrown@leemanlabs.com; Garry Kunselman
5:10 WS106 Innovative Sampling Techniques for Improving Productivity in Simultaneous CCD-Based ICP-AES. Michelle E. Cree, Varian, Inc., 13000 Weston Parkway, Cary NC 27513, michelle.cree@varianinc.com; Andrew Ryan
5:00 – 6:30 Social Mixer
Panel Discussion
5:30 PD02 Problems in Elemental Speciation. Maria Montes-Bayón, University of Oviedo, Department of Chemistry, C/Julian Claveria 8, E-33006 Oviedo, Spain, montesm@email.uc.edu; Joseph A. Caruso. Alfredo Sanz-Medel, Ryszard Lobinski, Jörg Bettmer, and Klaus G. Heumann
Wednesday, January 7, 2004
5. Laser Assisted Plasma Spectrochemistry
Gary M. Hieftje, Chair
08:00 PL03 Laser Assisted Plasma Spectrochemistry (Ablation). Richard E. Russo, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Mail Stop 70-193A, Berkeley CA 94720, rerusso@lbl.gov
09:00 IL08 The Future of Laser Ablation ICP Mass Spectrometry - ng or nm? Detlef Günther, Swiss Federal Institute of Technology, Laboratory of Inorganic Chemistry, Hönggerberg HCI G113, CH-8093 Zürich, Switzerland, guenther@inorg.chem.ethz.ch; Marcel Guillong
09:30 W01 Effect of Size, Chemical and Phase Composition of Ablated Particles on Elemental Fractionation During ICPMS Analysis. Jan Kosler, Charles University, Department of Geochemistry, Albertov 6, CZ-12843 Prague 2, Czech Republic, kosler@natur.cuni.cz; Michael Wiedenbeck, Richard Wirth, Jan Hovorka, Paul Sylvester, and Jitka Mikova
9:50 Break
10:10 W02 Birth, Life and Death of Laser-Induced Aerosols: Implications for the Elemental Analysis. Davide Bleiner, Federal Laboratories for Materials Research, EMPA, Überlandstrasse 129, CH-8600 Dübendorf, Switzerland, davide.bleiner@empa.ch
10:30 W03 Calibration and Particle Effects in Laser Ablation ICP-MS. David B. Aeschliman, Iowa State University, Ames Laboratory USDOE, Department of Chemistry, Ames IA 50011, macabre@iastate.edu; R.S. Houk, David Baldwin, and Stan Bajic
10:50 W04 Proteome Analysis of Alzheimer's Disease Target Proteins by FT-ICR-MS and Determination of Elements Concentrations by LA-ICP-MS. J. Susanne Becker, University of Konstanz, Department of Analytical Chemistry, AG Prof. Przybylski, Universtaets, D-78457 Konstanz, Germany, susanne.becker@uni-konstanz.de; Eugen Damoc, Myroslav Zoriy, Carola Pickhardt, and Michael Przyoylski
11:10 W05 Laser Ablation ICP-MS for the Detection of Phosphorelated Peptides. Fadi Abou-Shakra, GV Instruments, Crews Road, Wythenshawe, Manchester M23 9BE, United Kingdom, fadi.aboushakra@gvinstruments.co.uk; Victoria Elliott, Cameron McLeod, Peter Marshall, Kevin Reardon
11:30 W06 Analysis of Solids Using Laser Ablation ICP-OES with a Large Format Solid State Detector. Manny Almeida, Leeman Labs, Inc., 6 Wentworth Drive, Hudson NH 03051, malmeida@leemanlabs.com; Lawrence Neufeld
11:50 Lunch Break
Wednesday, January 7, 2004
6. Plasmas on a Chip, Spectroscopic Instrumentation
Vassali Karanassios, Chair
1:00 IL09 Inductively Coupled and Capacitively Coupled Microdischarges Operating in the UHF. Jeffrey A. Hopwood, Northeastern University, Electrical and Computer Engineering, 360 Huntington Avenue, Boston MA 02115, hopwood@ece.neu.edu
1:30 IL10 From the ICP to Microplasmas on a Chip. José A.C. Broekaert, University of Hamburg, Department of Chemistry, Martin-Luther-King-Platz 6, D-20146 Hamburg, Germany, jose.broekaert@chemie.uni-hamburg.de
2:00 W07 Development and Characterization of a Battery-Operated Plasma Device (MPD). Vassili Karanassios, University of Waterloo, Department of Chemistry, Waterloo ON N2L 3G1, Canada, vkaranassios@uwaterloo.ca; Andrea Smith, Kara Johnson
2:20 W08 Optical Design Considerations for a New Echelle VUV-VIS Spectrometer Designed for ICP-OES. Stan B. Smith Jr., Leeman Labs, Inc., 6 Wentworth Dr., Hudson NH 03051, pbrown@leemanlabs.com; Peter G. Brown, Art Reed, and Karl J. Hildebra
2:40 W09 ICP Imaging and Analytical Characteristics Using VIS and UV Acousto-Optic Tunable Filters. Jon Carnahan, Northern Illinois University, Department of Chemistry and Biochemistry, De Kalb IL 60115, carnahan@niu.edu; Ling Bei, Brian J. Englebert
3:00 – 6:30 Poster Session: Automation, Instrumentation, Laser Assisted Plasma Spectrometry, Software
Poster Session: New Instrumentation
WP01 Comparison of a Microstrip Plasma and a Miniaturized Radio-Frequency Plasma Source in Optical Emission Spectrometry. José A.C. Broekaert, University of Hamburg, Institute for Inorganic and Applied Chemistry, Martin-Luther-King-Platz 6, D-20146 Hamburg, Germany, jose.broekaert@chemie.uni-hamburg.de; Volker Siemens
WP02 The SPECTEC Family of Cleanroom Devices. Knut D. Ohls, Spetec GmbH, Justus-von-Liebig-Str. 2, D-85435 Erding, Germany, spetec-gmbh@t-online.de; F. Rickert
WP03 Determination of Nitrogen in Phosphate-Based Materials Using a New High Resolution ICP Equipped With a Large Format Programmable Array Detector. Garry Kunselman, Leeman Labs, Inc., 6 Wentworth Drive, Hudson NH 03051, gkunselman@leemanlabs.com; Peter Brown, Arthur Reed, and Manny Almeida
Poster Session: Laser Assisted Plasma Spectrometry
WP04 Isotope Dilution Laser Ablation ICP-MS for Direct Trace and Ultratrace Analysis of Environmental Samples. Sergei F. Boulyga, Johannes Gutenberg-University Mainz, Institute of Inorganic Chemistry and Analytical, Duesbergweg 10-14, D-55099 Mainz, Germany, boulyga@uni-mainz.de; Markus Tibi, and Klaus G. Heumann
WP05 Use of Laser Ablation for Analysis of Powdered Materials. Viktor Kanický, Masaryk University in Brno, Faculty of Science, Lab Atomic Spectrochemistry, Kotlarska 2, CZ-611 37 Brno, Czech Republic, viktork@chemi.muni.cz; Markéta Holá, Karel Novotný, Tomás Vaculovic, Vitezslav Otruba
WP06 UV-Femtosecond Laser Ablation - ICP-MS for Analysis of Alloy Samples. Jhanis González, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Mail Stop 108-D, Berkeley CA 94720, jjgonzalez@lbl.gov; Xinglei Mao, Chunyi Liu, and Richard Russo
WP07 Nanoparticles Differentiation in Laser-Ablation-Induced Aerosols: Implications for the Elemental Analysis of Si-Wafer. Davide Bleiner, Federal Laboratories for Materials Research-Switzerland, EMPA, Überlandstrasse 129, CH-8600 Dübendorf, Switzerland, davide.bleiner@empa.ch; Philippe Gasser, Peter Lienemann, Matthias Trottmann, and Andrea Ulrich
WP08 Micro-Homogeneity Considerations for the Forensic Analysis of Glass by Laser Ablation - ICP-MS. José R. Almirall, Florida International University, Department of Chemistry and Biochemistry, University Park, Miami FL 33199, almirall@fiu.edu; Tatiana Trejos, and Jeannette Perr
WP09 Characterization of Different New Glass Reference Material Using a Solid State 193 nm Nd:YAG Laser Ablation System. Marcel Guillong, ETH Swiss Federal Institute of Technology, Laboratory of Inorganic Chemistry, Hönggerberg HCI G107, CH-8093 Zürich, Switzerland, guillong@inorg.chem.ethz.ch; Detlef Günther
WP10 Effects of Thermal Treatment on Laser Generated Aerosols Using LA-ETV-ICP-MS. Marcel Guillong, ETH Swiss Federal Institute of Technology, Laboratory of Inorganic Chemistry, Hönggerberg HCI G107, CH-8093 Zürich, Switzerland, guillong@inorg.chem.ethz.ch; Jürg M. Binkert, and Detlef Günther
WP11 Applications of a Solid State Multiple Wavelength Laser Ablation System. Alan Koenig, CETAC Technologies, 14306 Industrial Road, Omaha NE 68144-3334, akoenig@cetac.com; Fred Smith, Joe Brady, and Bryan Carpenter
WP12 LA-ICP-MS -- Studies on the Ionization Efficiency of Laser-Induced Powder Samples. Ivana Kroslakova-Bindzarov, ETH Swiss Federal Institute of Technology, Laboratory of Inorganic Chemistry, Hönggerberg HCI G 107, CH-8093 Zürich, Switzerland, bindzarova@inorg.chem.ethz.ch; Detlef Günther
WP13 Particle-Size Related Elemental Fractionation of Glass: LA or ICP-MS? Hans-Rudolf Kuhn, ETH Zürich Laboratory of Inorganic Chemistry, ETH Hönggerberg HCI G111, Wolfgang-Pauli-Strasse 10, CH-8093 Zürich, Switzerland, kuhn@inorg.chem.ethz.ch; Detlef Günther
WP14 Diffusion Studies from a Cs Source into Bulk Rocks Using LA-ICP-MS and Synchrotron-Based Micro XRF. Detlef Günther, ETH Zürich, Laboratory of Inorganic Chemistry, Hönggerberg HCI G113, CH-8093 Zürich, Switzerland, guenther@inorg.chem.ethz.ch; Beat Aeschlimann, and Daniel Grolimund
WP15 Depth Profiling of Coated Metals by Laser Ablation-Inductively Coupled Plasma – Optical Emission Spectrometry. Viktor Kanicky, Masaryk University in Brno, Faculty of Science, Laboratory of Atomic Spectrochemistry, Kotlarska 2, CZ-611 37 Brno, Czech Republic, viktork@chemi.muni.cz; Ales Hrdlicka, Vitezslav Otruba
WP16 Depth-Profile Studies Using LA-ICP-MS. Viktor Kanicky, Masaryk University in Brno, Faculty of Science, Laboratory of Atomic Spectrochemistry, Kotlarska 2, CZ-611 37 Brno, Czech Republic, viktork@chemi.muni.cz; Hans-Ruedi Kuhn, and Detlef Günther
WP17 Studies of Laser Ablation - ICP Atomic Emission Spectrometry Using Laser Induced Plasma Emission Signals. Karel Novotny, Masaryk University in Brno, Faculty of Science, Laboratory of Atomic Spectrochemistry, Kotlarska 2, CZ-611 37 Brno, Czech Republic, viktork@chemi.muni.cz; Tomas Vaculovic, Viktor Kanicky, and Vitezslav Otruba
WP18 Sample Preparation Methods for Lead Concentration and Isotope Analysis in Pre-Anthropogenic Peat and Plant Material by Multi-Collector (MC-) and Laser Ablation (LA-) Inductively Coupled Plasma Mass Spectrometry (ICP-MS). Malin Kylander, Imperial College London, Department of Earth Science & Engineering, South Kensington Campus, London SW7 2AZ, United Kingdom, malin.kylander@imperial.ac.uk; Dominik Weiss, Bary Coles, and Teresa Jeffries
WP19 LA-ICP-MS of Human Hair. Eric Salin, McGill University, Department of Chemistry, 801 Sherbrooke St. W., Montreal QC H3A 2K6, Canada, eric.salin@mcgill.ca; Rebecca Lam, and Madeleine Jensen-Fontaine
WP20 Determination of Trace Elements in Fish Otoliths and Scales Using Solution Nebulization and Laser Ablation Double Focusing Sector Field Inductively Coupled Plasma Mass Spectrometry. Zhongxing Chen, Old Dominion University, Department of Chemistry and Biochemistry, 4541 Hampton Blvd, Norfolk VA 23529-0126, zchen@odu.edu; Cynthia M. Jones
WP21 Determination of Trace Metals in Dental Tissues by Laser Ablation - Inductively Coupled Plasma - Mass Spectrometry (LA-ICP-MS): A Quantification Attempt. Dula Amarasiriwardena, Hampshire College, School of Natural Science, Amherst MA 01002, dula@hampshire.edu; Aaron Buchsbaum, Socheata Tauch, Anahita Dua, Alan Goodman,
WP22 Semi Quantitative Analysis of Trace Metals in Over-the-Counter Calcium Supplements by Laser Ablation - Inductively Coupled Plasma - Mass Spectrometry (LA-ICP-MS). Dula Amarasiriwardena, Hampshire College, School of Natural Science, Amherst MA 01002, dula@hampshire.edu; Jeremy Draper, Faith Okpotor
WP23 LA-ICP-MS for Trace Element Determination in Thin Sections of Sediments. Carola Pickhardt and J. Sabine Becker, Research Centre Jülich GmbH, Central Department for Chemical Analysis, Postfach 1913, D-52425 Jülich, Germany, c.pickhardt@fz-juelich.de; Oliver Kranendonck, and Isaac B. Brenner
WP24 Determination of Uranium, Thorium and 235U/238U Isotopic Ratios at Trace and Ultratrace Quantities in Urine by LA-ICP-MS. Mechthid Burow, Research Centre Jülich, Department for Safety and Radiation Protection, Postfach 1913, D-52425 Jülich, Germany, m.burow@fz-juelich.de; Carola Pickhardt, Oliver Kranendonck, and J. Sabine Becker
WP25 Elemental Fractionation Studies on Matrix-Modified Lithium Tetraborate Pellets. Peter Weis, Universität des Saarlandes, Institute für Anorganische und Analytische Chemie und Radioch, Postfach 151150, D-66041 Saarbrücken, Germany, peter@newfallseason.de; Horst P. Beck, and Detlef Günther
WP26 Evaluation of Gemstones by Laser Ablation ICP-AES. Sergei Leikin, Spectro Analytical Instruments, Inc., 160 Authority Dr., Fitchburg MA 01420, sleikin@aol.com; George G. Glavin, Laurence Neufeld, and C.R. "Cap" Beesley
WP27 Recent Developments in Characterizing Semiconductor and Electronic Materials by Direct Solid Sampling ICP-MS. Fuhe Li, Balazs Analytical Services, Air Liquid America L.P., 46409 Landing Parkway, Fremont CA 94538, fli@balazs.com; Scott Anderson
WP28 Influence of Pulse Duration and Wavelength on Brass Sample Analysis by Laser Induced Plasma Spectroscopy (LIPS) Under Air Atmosphere. Vincent Detalle, National Research Council of Canada, Industrial Materials Institute, 75 Boul. de Mortagne, Boucherville QC J4B 6Y4, Canada, vincent.detalle@cnrc-nrc.gc.ca; M. Sabsabi, B. Le Drogoff, D. Menut, M. Chaker, J. Margot, F. Vidal, S. Laville, T.W. Johnston, and O. Barthélemy
WP29 Comparison of Interferences in Laser Induced Breakdown Spectroscopy, Inductively Coupled Plasma Spectroscopy, and Flame Spectroscopy. Scott R. Goode, University of South Carolina, Department of Chemistry and Biochemistry, Columbia SC 29208, goode@sc.edu; Jack E. Pender, Christopher R. Dockery, and Richard Hoskins
Poster Session: Automation, Software
WP30 Benefits of Integrating ICP-MS/OES Instruments with LIMS. Phil J. Goddard, CSols Inc., 220 Continental Drive, Suite 405, Newark DE 19713, philg@csols.com
WP31 Getting the "Right" Result. Phil J. Goddard, CSols Inc., 220 Continental Drive, Suite 405, Newark DE 19713, philg@csols.com
WP32 Sapphire – The Electronic Spectroscopy Software Package. Robert Forrest, Cavendish Instruments Ltd., West Mount, 463 Glossop Road, Sheffield S10 2QD, United Kingdom, Robert.forrest@cavendishinstruments.com
WP33 On Theory of Intellectual Analytical Machines. Egeniy D. Prudnikov and Evgeniy E. Prudnikov, St. Petersburg State University, Earth's Crust Institute, University emb. 7/9, St. Petersburg 199034, Russia, evgeniy@ep2256.spb.edu
WP34 Error and Uncertainty in Analysis. Egeniy D. Prudnikov, St. Petersburg State University, Earth's Crust Institute, University emb. 7/9, St. Petersburg 199034, Russia, evgeniy@ep2256.spb.edu
Workshop on New Plasma Instrumentation, Sample Preparation, and Accessories
Isaac (Joe) Brenner and Robert I. Botto, Chairs
Inductively Coupled Plasma –Mass Spectrometry
3:05 WS200 Setting the Scene - Challenges of Inductively Coupled Plasma Mass Spectrometry. Isaac (Joe) Brenner, Environmental Analytical Services, 9 Dishon Street, Apartment 9, Malkha, Jerusalem 96956, Israel, brenner@cc.huji.ac.il
3:10 WS201 Features and Performance of the 90 Degree Reflecting Ion Optics Varian ICP-MS. Shane Elliott, Varian Australia Pty Ltd, 679 Springvale Road, Mulgrave, Victoria 3170, Australia, shane.elliott@varianinc.com; Stephen Anderson, and Iouri Kalinitchenko
3:30 WS202 New Developments in Reaction Cell ICP-MS for Multi-Element Analysis in Unknown, Complex Matrix Samples. Abe G. Gutiérrez, Agilent Technologies, ICP-MS Sales and Support, 318 Indian Trace #250, Weston FL 33326, abe@agilenticpms.com
3:50 WS203 GV Instruments IsoProbe - Effective Combination of Collision Cell and High Mass Resolution. Zenon Palacz, GV Instruments, Crews Road, Wythenshawe, Manchester M23 9BE, United Kingdom, zenon.palacz@gvinstruments.co.uk; Patrick Turner, and Simon Meffan
4:10 WS204 Beyond Elemental Speciation: New Roles of Hyphenated ICP-MS in Elemental Detection Steve Wilbur, Agilent Technologies, 3380 146th Pl SE, Suite 300, Bellevue WA 98007-6472, steven_wilbur@agilent.com; Emmett Soffey, Raimund Wahlen, and Rudolf Grimm
4:30 WS205 ICP-MS Cones: Choices, Care and Cleaning. Bill Faulkner, Spectron, Inc., 2080 Sunset Drive, Ventura CA 93001, spectron@vcnet.com
4:50 WS206 Solving Difficult Sample Analysis Using ICP-MS – Performance of the Thermo Element 2 High Resolution Magnetic Sector ICP Mass Spectrometer. Meike Hamester, Thermo Electron (Bremen), Barkhausenstrasse 2, D-28197 Bremen, Germany, meike.hamester@thermo.com
5:00 – 6:30 Social Mixer
Panel Discussion
5:30 PD03 Direct Solid Sample Analysis by Means of Laser Probes: Breakthrough or Breakdown? Davide Bleiner (chair), Swiss Federal Laboratories for Materials Testing and Research, Überlandstrasse 129, CH 8600 Dübendorf, Switzerland; panelists Annemie Bogaerts (Antwerpen), Marcel Guillong (Zürich), Jan Kosler (Prague), Nicolň Omenetto (Gainesville), and Richard Russo (Berkeley); davide.bleiner@empa.ch
Thursday, January 8, 2004
7. Excitation Mechanisms and Plasma Phenomena
Nicolň Omenetto, Chair
08:00 PL04 Prognosis for Plasma-Source Mass Spectrometry. Gary M. Hieftje, Indiana University, Department of Chemistry, 800 E. Kirkwood Avenue, Bloomington IN 47405-7102, hieftje@indiana.edu; Francisco Andrade, James H. Barnes, IV, Denise M. McClenathan, Steven J. Ray, Duane A. Rogers, Gregory D. Schilling, William C. Wetzel, M. Bonner Denton, David W. Koppenaal, and Charles Baranage
09:00 IL11 Laser Ablation: Can Modeling Help Us to "See the Light"? Annemie Bogaerts, University of Antwerp (UIA), Department of Chemistry, Universiteitsplein 1, B-2610 Wilrijk - Antwerp, Belgium, annemie.bogaerts@ua.ac.be; Zhaoyang Chen
09:30 IL12 Is the Availability of the Entire UV-Visible Emission Spectrum Beneficial to Our Understanding of the ICP? Jean-Michel Mermet, Unversité Claude Bernard - Lyon I, Laboratoire des Sciences Analytiques, Batiment -CPE, F69622 Villeurbanne Cedex, France, mermet@cpe.fr
10:00 Break
10:20 Th01 Chemical Imaging Laser Ablation ICP-MS. Christopher Latkoczy, ETH Zürich Laboratory of Inorganic Chemistry, Hönggerberg HCI G111, Wolfgang-Pauli-Strasse 10, CH-8093 Zürich, Switzerland, latkoczy@inorg.chem.ethz.ch; Detlef Günther
10:40 Th02 Fundamental Characterization of a Planar-Cathode Glow Discharge: Parametric Observations via Laser-Scattering Techniques and Computer Modeling. Gerardo Gamez, Indiana University, Department of Chemistry, Bloomington IN 47405, ggamez@indiana.edu; Francisco Andrade, Gary M. Hieftje, and Annemie Bogaerts
11:00 Th03 GDMS: Ionisation of Rydberg Species at the Plasma Boundary. Rod S. Mason, University of Wales Swansea, Department of Chemistry, Singleton Park, Swansea SA2 8PP, United Kingdom, r.s.mason@swan.ac.uk; Ifor P. Mortimer, Dylan R. Williams, and David J. Mitchell
11:20 Th04 High-Resolution Images of the Sampling Cone of an Inductively Coupled Plasma Mass Spectrometer. Paul B. Farnsworth, Brigham Young University, Department of Chemistry and Biochemistry, C100 Benson Science Building, Provo UT 84602-5700, paul_farnsworth@byu.edu; Jeffrey H. Mcedone and Andrew A. Mills
11:40 Th05 Investigation and Alleviation of Analyte-Oxide Interferences by Inductively Coupled Plasma Time-of-Flight Mass Spectrometry. William C. Wetzel, Indiana University, Department of Chemistry, Bloomington IN 47405, wwetzel@indiana.edu; Denise M. McClenathan, and Gary M. Hieftje
12:00 Lunch Break
Thursday, January 8, 2004
8. Sample Preparation, Treatment, and Analysis
Skip Kingston, Chair
1:00 IL13 Is an Improvement in the Field of Sample Decomposition Still Imaginable? Günter Knapp, Graz University of Technology, Institute of Analytical Chemistry, Micro- and Radiochemistry, Technikerstrasse 4, A-8010 Graz, Austria, knapp@analytchem.tu-graz.ac.at
1:30 Th06 Combination of a New High-Throughput Rotor and Diluted Acid for Closed-Vessel Microwave-Assisted Digestion of Biological Materials. Joaquim Nóbrega, Universidade Federal de Săo Carlos, Depto Quimica, Caixa Postal 676, Săo Carlos, SP 13565-905, Brazil, djan@terra.com.br; Clésia C. Nascentes, Geórgia C.L. Araújo, Ana Rita A. Nogueira, and Camillo Pirola
1:50 Th07 Microwave Digestion of High Temperature Refractory Materials with Subsequent HF Elimination by Microwave-Assisted Evaporation with Temperature Cutoff. Bob Lockerman, CEM Corporation, P.O. Box 200, 3100 Smith Farm Rd., Matthews NC 28106-0200, nicole.collins@cem.com; Elaine Hasty
2:10 Th08 Novel Methods in High Throughput and High Purity Microwave Sample Preparation. Peter Kainrath, S-prep GmbH, Im Amann 7, D-88662 Überlingen 7, Germany, kainrath@s-prep.com; Peter Kettisch, and Michael Zischka
2:30 Th09 Enabling Speciated Isotope Dilution Mass Spectrometry for Difficult Species Sample Preparation and Analysis. H.M. "Skip" Kingston, Duquesne University, Department of Chemistry and Biochemistry, Center for Environmental Research, Pittsburgh PA 15282-1530, kingston@duq.edu; Mizanur Rahman, John Kern, Matt Pmuku, Karin Rosen, Ye Han, Dingwei Huo, and Theo Towns
3:00 – 6:30 Poster Session: Applications, Glow Discharge Atomic/Mass Spectrometry, Mechanisms and Diagnostics, Plasma Sources, Sample Preparation and Standards, Teaching Spectroscopy
Poster Session: Plasma Spectrochemical Analysis
ThP01 Spectral Interference Correction in ICP-AES Using Artificial Neural Networks. Vassili Karanassios, University of Waterloo, Department of Chemistry, Waterloo ON N2L 3G1, Canada, vkaranassios@uwaterloo.ca; Zhimin Li
ThP02 Practical Approach to Selection of Internal Standards for Correction of Nonspectral Interferences in ICP-AES Analysis. Natalie Kutsen, RSR Technologies, Inc., 2804 Sea Harbor Rd., Dallas TX 75212, nkutsen@rsrtechnologies.com; Andreas Siegmund
ThP03 High-Resolution ICP-OES Analysis of Zirconium Metal. Geoff Tyler, Jobin Yvon SAS, 16-18, rue du Canal, F-91165 Longjumeau Cedex, France, geoftyler@aol.com; Agnčs Cosnier, Nathalie Le Corre, Sébastien Velasquez, Desirée Ahlum, and Albert Brennsteiner
ThP04 Determination of Trace Elements in Precious Metals by ICP-OES. Geoff Tyler, Jobin Yvon SA, 16-18, rue du Canal, F-91165 Longjumeau Cedex, France, geoftyler@aol.com; Agnčs Cosnier, Nathalie Le Corre, Celia Olivero, Desirée Ahlum, and Albert Brennsteiner
ThP05 Emission Spectrometric Determination of Boron in Graphite Material with the Axial Plasma Source. Jarmila Lastincová, Slovak University of Technology, Department of Analytical Chemistry FCHPT-STU, Radlinskeho 9, SK-812 37 Bratislava, Slovakia, lastin@chelin.chtf.stuba.sk; Ernest Beinrohr, Viera Siranová, L'ubica Popísilová
ThP06 Flexible Procedure for Steel Analysis by ICP-OES. Myriam V. Moreno López, Research Center in Advanced Materials, Miguel de Cervantes 120, Complejo Industrial Chihuahua, Chihuahua, Chih. C.P. 31109, México, miriam.moreno@cimav.edu.mx; Aida Álvarez Alonso, and Siliva V. Miranda Navarro
ThP07 Determination of Iodine in Biological and Food Samples by ICP-OES in VUV. Viktor Kanicky, Masaryk University in Brno, Faculty of Science, Laboratory of Atomic Spectrochemistry, Kotlarska 2, CZ-611 37 Brno, Czech Republic, viktork@chemi.muni.cz; Eva Niedobová, Jiri Machát, and Vitezslav Otruba
ThP08 Utilization of Hydride Generation Technique for the Determination of Selenium, Arsenic, Antimony and Tellurium. Viktor Kanicky, Masaryk University in Brno, Faculty of Science, Laboratory of Atomic Spectrochemistry, Kotlarska 2, CZ-611 37 Brno, Czech Republic, viktork@chemi.muni.cz; Jitka Studynková, Jiri Machát, and Vitezslav Otruba
ThP09 Analysis of Agricultural Samples by Simultaneous ICP-OES. Michelle E. Cree, Varian, Inc., 13000 Weston Parkway, Cary NC 27513, michelle.cree@varianinc.com; Christine Rivera
ThP10 Spectrometric Methods Used for Determination of Heavy Metals in Accidental Polluted Soils. Vasile Viman, North University of Baia Marie, Victor Babes Street No 62A, 4800 Bai Mare, Romania, v_viman@hotmail.com; Anca Mihaly Cozmuta, Leonard Mihaly Cozmuta, Mariana Dobra, Gheorghe Vatca
ThP11 Determination of Nitrogen in Fertilizers by ICP-AES. George G. Glavin, Spectro Analytical Instruments, Inc., 160 Authority Dr., Fitchburg MA 01420, ggglavin@spectro-usa.com; Sergei Leikin
ThP12 New Life for a Vintage Spectrometer – Application to the Analysis of Soil Leachates. Graeme A. Spiers, Laurentian University, Centre for Environmental Monitoring, MIRARCO, Sudbury, ON Canada; gspiers@mirarco.org
Poster Session: Sample Preparation and Standards, Pure Materials
ThP13 Trace Element Analysis of Diesel Vehicle Emissions by ICP-MS. Andrea Ulrich, EMPA, Swiss Federal Laboratories for, Materials Testing and Research, Überlandstrasse 129, CH-8600 Dübendorf, Switzerland, andrea.ulrich@empa.ch; Adrian Wichser
ThP14 Application of HR-ICPMS for Multi-Element Determination in Aerosol Particles Collected at "High Traffic Locations" in Europe. Petra Krystek, National Institute of Public Health and Environment RIVM, Laboratory for Analytical Chemistry, P.O. Box 1, NL-3720 BA Bilthoven, The Netherlands, petra.krystek@rivm.nl; Rob Ritsema
ThP15 ICP-MS Analysis of Wood Cores from The Kiawe Tree (Prosopis pallida): Can Environmental Trends in Hawaii be Reconstructed from Trace Element Distributions? Eric Heinen De Carlo, University of Hawaii, Department of Oceanography SOEST, 1000 Pope Rd., MSB 510, Honolulu HI 96822, edecarlo@soest.hawaii.edu; Yvonne Katrin Parry, Steven R. Spengler, and Matthew Neal
ThP16 Beryllium Detection in Workplace Swipes by Inductively Coupled Plasma Mass Spectrometry. Charles R. Shick, Jr., Savannah River Technology Center, Building 735-A, D-171, Aiken SC 29803, charles.shick@srs.gov; Paula R. Cable-Dunlap, and Stephen P. LaMont
ThP17 A Novel On-Line Sequential Extraction Procedure for Metal Partitioning in Soils and Sediments. Steve J. Hill, University of Plymouth, Department of Environmental Sciences, Drake Circus, Plymouth Devon PL4 8AA, United Kingdom, sjhill@plymouth.ac.uk; Rebeca Santamaria-Fernández, and Mark R. Cave
ThP18 Use of a Novel Sequential Extraction Procedure and Chemometric Data Treatment to Asses the Metal Distribution Within the Physico-Chemical Components in Sediments from the Galician Coast (N.W. Spain). Steve J. Hill, University of Plymouth, Department of Environmental Sciences, Drake Circus, Plymouth Devon PL4 8AA, United Kingdom, sjhill@plymouth.ac.uk; Rebeca Santamaria-Fernández, and Mark R. Cave
ThP19 Determination of Phosphorus in Polymeric Systems Using Ashing Procedure and ICP-AES. Antoaneta P. Krushevska, General Electric Global Research, One Research Circle, Bldg. K-1Room 2A 28, Niskayuna NY 12309, krushevska@crd.ge.com; June Klimash, Joanne F. Smith, Patrick J. McCloske, and Elizabeth A. Williams
ThP20 Improved Elemental Recoveries in Soils with H3BO3 Heating During Microwave Digestion. Rebecca Burt, USDA - Natural Resources Conservation Service, Soil Survey Laboratory, 5111 West Sumner Circle, Lincoln NE 68522, rebecca.burt@nsscnt.nssc.nrcs.usda.gov; Michael A. Wilson, Chris W. Lee, and Richard Ferguson
ThP21 Ultrapure Water Quality and ICP-MS Applications. Stéphane Mabic, Millipore, Laboratory Water Division, R&D, BP 307, F-78054 Saint-Quentin Yvelines, France, stephane_mabic@millipore.com
ThP22 Ultrapure Water for Elemental Analysis Down to ppt Level.. Stéphane Mabic, Millipore, Laboratory Water Division, R&D, BP 307, F-78054 Saint-Quentin Yvelines, France, stephane_mabic@millipore.com; Ichiro Kano, and Daniel Darbouret
ThP23 Lab Accessories Related Contamination: Fact or Fiction? Andrea Wichser, EMPA, Swiss Federal Laboratories for, Materials Testing and Research, Überlandstrasse 129, CH-8600 Dübendorf, Switzerland, adrian.wichser@empa.ch; G. Mueller, C. Schreiner, and R. Figi
ThP24 Errors Generated During Lead and Thallium Isotope Analysis by MC-ICP-MS: A Result of Analyte Ions Interaction in Solution. George D. Kamenov, University of Florida, Department of Geological Sciences, 241 Williamson Hall PO Box 112120, Gainesville FL 32611, kamenov@ufl.edu; Paul A. Mueller, Michael R. Perfit, and Ann L. Heatherington
ThP25 Comparison of Sample Preparation Techniques of Serum Samples for ICP-MS Analysis. Peter J. Walter, Batelle Memorial Institute, Atlanta GA 30341, klc7@cdc.gov; Kathleen L. Caldwell, and Robert L. Jones
Poster Session: Glow Discharge Atomic and Mass Spectrometry
ThP26 The Addition of H2 to an Ar Plasma Studied by Fast Flow Glow Discharge Mass Spectrometry (FFGD-MS): Mechanism and Relative Sensitivities. Karla Newman, University of Wales Swansea, Department of Chemistry, Singleton Park, Swansea SA2 8PP, United Kingdom, karla_newman@isic.org; Rod S. Mason
ThP27 Survey on the Suitability of Coatings Containing Hydrogen as Layered CRM for GD-OES. Vasile-Dan Hodoroaba, Federal Institute for Materials Research, and Testing (BAM), Unter den Eichen 87, D-12205 Berlin, Germany, dan.hodoroaba@bam.de; Volker Hoffmann and Wolfgang Paatsch
ThP28 Novel Use of Sol-Gels as Solid Matrices for Simultaneous Multi-element Determination by Radio Frequency Glow Discharge Optical Emission Spectrometry: Determinations of Suspended Particulate Matter. Timothy M. Brewer, Clemson University, Department of Chemistry, 102 BRC Laboratory, Clemson SC 29634-0973, tbrewer@clemson.edu; Julia E. Cooper, Wandee Luesaiwong, Brian K. Sprual, R. W. Clay Davis, and R. Kenneth Marcus
ThP29 Polypeptide and Nucleobase Spectral Features in Particle Beam Glow Discharge Mass Spectrometry. Jacob L. Venzie, Clemson University, Department of Chemistry, 102 BRC Laboratory, Clemson SC 29634-0973, jvenzie@clemson.edu; W. Clay Davis, Timothy Brewer, R. Kenneth Marcus
ThP30 Investigation of Potential Carrier Effects in the Application of Particle Beam/Hollow Cathode-Optical Emission Spectroscopy (PB/HC-OES) for Total Protein Determinations Based on Atomic Carbon Responses. Fuxia Jin, Clemson University, Department of Chemistry, 235 Howard L. Hunter Laboratory, Clemson SC 29634-0973, fjin@clemson.edu; Keith Lenghaus, James J. Hickman, and R. Kenneth Marcus
ThP31 Multi-elemental Screening of Soils by Direct Current Glow Discharge Mass Spectrometry. Stéphane Baude, Commissariat ŕ l’Energie Atomique, Service Radioanalyse, Chimie, Environnement, BP 12, F-91680 Bruyčres-le-Chatel, France, stephane.baude@cea.fr; Patrick Andres, and Fabien Pointurier
ThP32 Internal Standard Addition Glow Discharge Mass Spectrometry for the Determination of Radionuclides. Maria Betti, Institute for Tansuranium Elements, Joint Research Centre - European Commission, P.O. Box 2340, D-76125 Karlsruhe, Germany, betti@itu.fzk.de; Ramon Carlos Marquez, and L. Aldave de las Heras
ThP33 Parametric Study of a Radiofrequency Glow Discharge Used for Optical Emission Spectroscopy. Laurent Therese, Centre de Physique des Plasmas CPAT, UMR 5002, 118, route de Narbonne, F-31062 Toulouse Cedex 4, France, belenguer@cpat.ups-tlse.fr; Philippe Guillot, and Philippe Belenguer
ThP34 Characterization of Surfaces and Thin Films Down to the Nanometer Scale of Conductive and Non-Conductive Materials by RF-GD-OES. Patrick Chapon, Jobin Yvon SAS, 16-18 rue du canal, F-91165 Longjumeau cedex, France, chaponp@aol.com; Richard Payling, Celia Olivero, and Philippe Hunault
ThP35 New Developments in RF Glow Discharge Optical Emission Spectrometry Extends the Range of Applications. Patrick Chapon, Jobin Yvon SAS, 16-18 rue du canal, F-91165 Longjumeau cedex, France, chaponp@aol.com; Richard Payling, Celia Olivero, Olivier Bonnot, Philippe Hunault
ThP36 Calculation of the Cathode (Sample) Temperature in Analytical Glow Discharges. Annemie Bogaerts, University of Antwerp (UIA), Department of Chemistry, Universiteitsplein 1, B-2610 Wilrijk - Antwerp, Belgium, annemie.bogaerts@ua.ac.be; Renaat Gijbels
Poster Session: Plasma Mechanisms and Diagnostics
ThP37 Use of Source Modulation Techniques in Inductively Coupled Plasma Time-of-Flight Mass Spectrometry. Denise McClenathan, Indiana University, Department of Chemistry, Bloomington IN 47405, dmcclena@indiana.edu; William C. Wetzel, and Gary M. Hieftje
ThP38 Using Matrix Effects as a Probe for the Study of the Charge-Transfer Excitation Mechanism in Inductively Coupled Plasma - Atomic Emission Spectrometry. George C.-Y. Chan, Indiana University, Department of Chemistry, Bloomington IN 47405, hieftje@indiana.edu; Gary M. Hieftje
ThP39 Spectroscopic Measurements of Plasma Properties in an Air-Cooled Argon/Helium ICP. Hidekazu Miyahara, Tokyo Institute of Technology, Department of Energy Sciences, 4259 Nagatsuta, Modori-ku, Yokohama 226-8502, Japan, miya@hotta.es.titech.ac.jp; Takayuki Doi, Youichi Mizusawa, Yasushi Hayashi, Eiki Hotta, Akitoshi Okino
ThP40 A Novel Setup to Investigate the Plasma Conditions in DSI-ICP-AES. Andy W.K. Cheung, The University of Hong Kong, Department of Chemistry, Pokfulam Road, Hong Kong, China, h9742954@graduate.hku.hk; W.T. Chan
ThP41 Direct Droplet Imaging for Two-Dimensional Aerosol Characterization in Inductively Coupled Plasmas. Kaveh Kahen, Kaveh Jorabchi, The George Washington University, Department of Chemistry, 725 21st St., NW, Washington DC 20052; Callium Gray, Jonathan A. Levine, and Akbar Montaser, kavehj@gwu.edu, kahen@gwu.edu, montaser@gwu.edu
Poster Session: Plasma Sources
ThP42 Trace Element Analysis by Sliding Spark Spectrometry. Hudson K. Angeyo, Universität Duisburg - Essen, Institute für Chemie, FG Instrumentelle Analytik, D-47048 Duisburg, Germany, angyo@lims.uni-duisburg.de; Alfred Golloch, S. Brockes
ThP43 Spectral Diagnostics of the Sliding Spark Plasma. Hudson K. Angeyo, Universität Duisburg - Essen, Institute für Chemie, FG Instrumentelle Analytik, D-47048 Duisburg, Germany, angyo@lims.uni-duisburg.de; Alfred Golloch, S. Brockes
Poster Session: Teaching Spectroscopy
ThP44 Research Based Analytical Chemistry Course: Opportunities, Pedagogical Advantages and Rewards. Dula Amarasiriwardena, Hampshire College, School of Natural Science, Amherst MA 01002, dula@hampshire.edu
Workshop on New Plasma Instrumentation, Sample Preparation, and Accessories
Isaac (Joe) Brenner and Robert I. Botto, Chairs
Direct Solids Analysis – Laser Ablation
3:00 WS300 Setting the Scene – Challenges for Direct Sample Analysis vs. Sample Preparation. Robert I. Botto, ExxonMobil Chemical Company, Baytown Chemical Plant Laboratory, 4500 Bayway Drive, Baytown TX 77520, bob.i.botto@exxonmobil.com
3:10 WS301 Laser Ablation Solid Sampling for Plasma Spectrochemistry: The Importance of Matching the Hardware to the Application. Lawrence Neufeld, New Wave Research Inc., 47613 Warm Springs Blvd, Fremont CA 94539, lneufield@new-wave.com; John Roy
Sample Preparation
3:30 WS302 Use of NIST High Performance Method for Certifying Commercial Standards. Tom Rettberg, VHG Labs, Inc., 276 Abby Road, Manchester NH 03103, trettberg@vhglabs.com; Susan Evans-Norris, J. MacIntosh, and J. Dupont
3:50 WS303 Achieving Accuracy in the Determination of ppb and ppt Range Concentration of Metals by ICP/ICPMS. Ralph Obenauf, SPEX CertiPrep, Inc., 203 Norcross Avenue, Metuchen NJ 08840, robenauf@spexcsp.com; Nimi Kocherlakota
4:10 WS304 Advanced Clean Chemistry Techniques for Controlling the Analytical Blank in Trace Analysis. Roy Mirchandani, Milestone Inc., 160B Shelton Road, Monroe CT 06468, rgm@milestonesci.com; Merrill Loechner
4:30 WS305 Comparative Study of Three Wet Digestion Techniques Using Three Distinct Temperature Programs with Analysis by Inductively Coupled Plasma-Atomic Emission Spectrometer (ICP-AES). Ranjan Roy, SCP SCIENCE, 348 Route 11, Champlain NY 12919-4816, rroy@scpscience.com; Gaston Mercier, and Laurie H.M. Chan
Panel Discussion
5:00 TS01 Teaching Analytical Atomic Spectroscopy: An International Perspective. Vassili Karanassios, University of Waterloo, Department of Chemistry, Waterloo ON N2L 3G1, Canada, vkaranassios@uwaterloo.ca; Detlef Günther, Jean-Michel Mermet, José Broekaert, and Alfredo Sanz-Medel
6:30 Conference Dinner
Friday, January 9, 2004
9. Plasma Source Mass Spectrometry: Fundamentals and Instrumentation
Paul Farnsworth, Chair
08:00 PL05 Plasma Source Mass Spectrometers: Sources and Developments. Norbert Jakubowski, Institute for Spectrochemistry, and Applied Spectroscopy, P.O. Box 10 13 52, D-44013 Dortmund, Germany, jakubowski@isas-dortmund.de; Joachim Franzke, and Kai Niemax
09:00 IL14 ICP-MS Instrumentation: Status and Future. R.Sam Houk, Iowa State University, Department of Chemistry, Ames Laboratory-USDOE, Ames IA 50011-3020, rshouk@iastate.edu, macabre@iastate.edu; David B. Aeschliman, F. Li, and J.W. Ferguson
09:30 IL15 Progress in Collision Cell ICP-MS: Recipe Collections and Science. Gregory Eiden, Battelle, Pacific Northwest National Laboratory, Richland WA 99352, gregory.eiden@pnl.gov; Charles J. Barinaga, and David W. Koppenaal
10:00 Break
10:20 F01 Ion-Molecule Reactions with Analyte and Overlap Ions for Simple and Complex Sample Analysis by ICP-MS. John W. Olesik, The Ohio State University, Department of Geological Sciences, 125 S. Oval Mall, Columbus OH 43210, olesik.2@osu.edu; Deanne R. Jones
10:40 F02 Description of Ion Energy and Collisional Relaxation in Reaction Cell. Vladimir I. Baranov, MDS SCIEX, 71 Four Valley Drive, Concord, ON L4K 4V8, Canada, vladimir.baranov@sciex.com
11:00 F03 Can Dynamic Reaction Cell ICP-MS Be Used for Multielement Analysis of Geoenvironmental Samples? Optimization of Operating Conditions and Validation. Michael Zischka, Technical University Graz, Institute for Analytical Chemistry, Micro and Radiochemistry, Technikerstrasse 4, A-8010 Graz, Austria, zischka@analytchem.tu-graz.ac.at; Günther Knapp, Isaac (Joe) B. Brenner
11:20 F04 The Science of Ion-Molecule Chemistry Recipes in ICP-MS. Dmitry R. Bandura, PerkinElmer-SCIEX, 71 Four Valley Drive, Concord, ON L4K 4V8, Canada, dmitry.bandura@sciex.com; Vladimir I. Baranov, and Scott D. Tanner
11:40 F05 Novel Array Detector Coupled to an Inductively Coupled Plasma Mass Spectrograph for the Detection of Transient Chromatographic Signals. Gregory D. Schilling, Indiana University, Department of Chemistry, 800 E. Kirkwood Avenue, Bloomington IN 47405-7102, gschilli@indiana.edu; James H. Barnes IV, Gary M. Hieftje, Roger Sperline, M. Bonner Denton, Charles J. Barinaga, and David W. Koppenaal
12:00 Lunch Break
Friday, January 9, 2004
10. Plasma Source Mass Spectrometry: Applications and Instrumentation
Ken Marcus, Chair
1:00 IL16 Increasing Use of the Glow Discharge for Both Atomic and Molecular Analysis. Willard W. Harrison, University of Florida, Department of Chemistry, 354 Leigh Hall, Gainesville FL 32611, harrison@chem.ufl.edu; Kevin Turney, Elizabeth Hastings
1:30 IL17 Application of GDMS in Different Fields of Research in Comparison to Other Analytical Techniques. Maria Betti, Institute for Tansuranium Elements, European Commission, JRC, P.O. Box 2340, D-76125 Karlsruhe, Germany, betti@itu.fzk.de; Laura Aldave de las Heras
2:00 F06 Investigation of Ultra-Thin Layers by RF-GD-OES. Volker Hoffmann, Leibniz Institute for Solid State and, Materials Research Dresden, P.O. Box 27 00 16, D-01171 Dresden, Germany, v.hoffmann@ifw-dresden.de; Rene Huebner, Michael Hecker, Stefan Baunack, Norbert Mattern, Klaus Wetzig, and Rainer Groetzschel
2:20 F07 The Hydrogen Effect in GD-OES Revisited -- Investigations of Polymer Coatings. Arne Bengtson, Swedish Institute for Metals Research, Drottning Kristinas väg 48, S-114 28 Stockholm, Sweden, gds@simr.se; Thomas Björk
2:40 F08 A Comparison of Relative Sensitivity Factors for rf and dc Sources for Glow Discharge Mass Spectroscopy. M. LeRoy Jacobs, Wyoming Analytical Laboratories, Inc., 1511 Washington Avenue, Golden CO 80401, walxray@aol.com; Charles R. Wilson, and Mark R. O'Brien
3:00 – 6:30 Poster Session
Poster Session: Plasma Mass Spectrometry Applications, Fundamentals, Instrumentation, Stable Isotopes
FP01 Octapole Reaction System ICPMS for the Determination of Selenium in Serum -- Theory, Development and Application. Stefan Stürup, Dartmouth College, Dartmouth Trace Element Core Facility, 6105 Sherman Fairchild Hall, Hanover NH 03755-3571, stefan.sturup@dartmouth.edu
FP02 A Calibration Method for Liquid Chromatography - Inductively Coupled Plasma - Mass Spectrometry. Eric Salin, McGill University, Department of Chemistry, 801 Sherbrooke St. W., Montreal QC H3A 2K6, Canada, eric.salin@mcgill.ca; Margaret Antler, Jane Maxwell
FP03 The Analysis of High and Low K Materials by ICP-MS. Tracey Jacksier, Air Liquide, Chicago Research Center, 5230 S. East Ave., Countryside IL 60525, tracey.jacksier@airliquide.com; Janet Graehling
FP04 Determination of Silicon in Aqueous and Organic Samples by DRC-ICP-MS. Katsu Kawabata, PerkinElmer Life & Analytical Sciences, 71 Four Valley Dr., Concord ON L4K 4V8, Canada, katsu.kawabata@sciex.com; Yoko Kishi, and Osamu Shikino
FP05 Reduction of Hafnium, Zirconium and Titanium Oxide, Hydroxide and Doubly Charge Interface Ions by DRC-ICP-MS. Yoko Kishi, PerkinElmer Life & Analytical Sciences, 71 Four Valley Dr., Concord ON L4K 4V8, Canada, yoko.kishi@sciex.com; Katsu Kawabata, and Osamu Shikino
FP06 Determination of Phosphorus and Sulfur by DRC-ICP-MS. Kenneth R. Neubauer, PerkinElmer Life and Analytical Sciences, 710 Bridgeport Avenue, Shelton CT 06484-4794, kenneth.neubauer@perkinelmer.com
FP07 Eclectic Unpublished Results in ICP-MS. Scott Tanner, PerkinElmer Sciex, 71 Four Valley Drive, Concord, ON L4K 4V8, Canada, scott.tanner@sciex.com
FP08 The Application of Collision/Reaction Cell ICP-MS to the Analysis of Variable and Unknown Samples Without Requiring Matrix-Specific or Element-Specific Tuning and Cell Conditions. Edward McCurdy, Agilent Technologies UK Ltd, Life Sciences and Chemical Analysis, Lakeside, Cheadle Royal Business, Stockport, Cheshire SK8 2GR, United Kingdom, ed_mccurdy@agilent.com; Don Potter, Glenn Woods, and Steve Wilbur
FP09 The Effect of Interface Design on Matrix Effects in ICP-MS: Part 1. Phil Shaw, Thermo Elemental Corporation, Ion Path, Road Three, Winsford, Cheshire CW7 3BX, United Kingdom, phil.shaw@thermo.com; Jonathan Batey, Bill Spence
FP10 Direct Analysis of Seawater by Collision Cell ICP-MS. Bill Spence, Thermo Elemental, Ion Path, Road Three, Winsford, Cheshire CW7 3BX, United Kingdom, bill.spence@thermo.com; Simon Nelms, Martin Nash, and Jonathan Batey
FP11 Novel ICP-MS Applications for Clinical Sample Analysis. Bill Spence, Thermo Elemental, Ion Path, Road Three, Winsford, Cheshire CW7 3BX, United Kingdom, bill.spence@thermo.com; Simon M. Nelms, and Martin Nash
FP12 Mixed-Mode, Multi-Element Urine Analysis by ICP-DRC-MS. Jeffery M. Jarrett, Centers for Disease Control & Prevention, 4770 Buford Hwy NE, Mail Stop F-18, Atlanta GA 30341-3724, jhj8@cdc.gov; Ge Xiao, Kathy L. Caldwell, and Robert L. Jones
FP13 Comparison of ICP-OES vs. ICP-DRC-MS Analysis of Copper and Zinc in Serum Samples. Peter J. Walter, Battelle Memorial Institute, Atlanta GA 30341, pwalter@cdc.gov; Amir Makhmudov, Kathleen L. Caldwell, and Robert L. Jones
FP14 Concentrations of 18 Elements in Whole Blood and Serum for Southern Nevada Wild Horses by Sector-Field ICPMS. James V. Cizdziel, University of Nevada Las Vegas, Harry Reid Center for Environmental Studies, 4505 Maryland Parkway, Las Vegas NV 89154-4009, cizdziej@unlv.edu; Susan Meacham
FP15 A Pilot Study on the Release of Metal Ions from Hip Arthroprothesis. Sergio Caroli, Istituto Superiore di Sanitŕ, Viale Regina Elena 299, I-00161 Rome, Italy, caroli@iss.it; I. Iavicoli, G. Carelli, S. Salvatori, G. Falcone, M. Alessandrelli, and R. Cresti
FP16 A Dual-Source Inductively Coupled Plasma/Electrospray Ionization Time-of-Flight Mass Spectrometer for the Simultaneous Acquisition of Atomic and Molecular Mass Spectra. Steven J. Ray, Indiana University, Department of Chemistry, Bloomington IN 47405, sjray@indiana.edu; Duane Rogers, and Gary M. Hieftje
FP17 Better ICP-MS Stability for Difficult Samples. Michael Plantz, Varian, Inc., 201 Hansen Court, Suite 108, Wood Dale IL 60191, mike.plantz@varianinc.com; Steve Anderson, Shane Elliott, Iouri Kalitchenko
FP18 A Novel Plasma Interface for ICP-MS. Iouri Kalinitchenko, Varian Australia Pty Ltd, 679 Springvale Road, Mulgrave, Victoria 3170, Australia, shane.elliott@varianinc.com
FP19 Enhancing the Sensitivity of Elemental Fourier Transform Ion Cyclotron Resonance Mass Spectrometry for Low Abundance Ions. Keith D. Zientek, University of Florida, Department of Chemistry, PO Box 1172000, Gainesville FL 32601-7200, kzientek@chem.ufl.edu; John R. Eyler
FP20 Variations in Instrumental Mass Discrimination in MC-ICPMS. Henrik Andrén, Luleĺ University of Technology, Divisions of Chemistry, S-971 87 Luleĺ, Sweden, henrik.andren@km.luth.se; Douglas C. Baxter, Anna Stenberg, Dmitry Malinovsky, and Ilia Rodushkin
FP21 Analyzing ppt and ppq Levels of Impurities in High Purity Acids and Water. Brad McKelvey, Seastar Chemicals, Inc., P.O. Box 2219, 10005 McDonald Park Road, Sidney BC V8L 3S8, Canada, bmckelvey@axys.com; David MacLeod and Shelley McIvor
FP22 Low-Level Chromium Measurements in Human Samples by Sector Field ICP-MS. Joachim Hinrichs, Thermo Electron, 2 Barkhausenstrasse, D-28197 Bremen, Germany, joachim.hinrichs@thermo.com; Andreas Guensel
FP23 Retention of Cr(III) by High-Performance Chelation Ion Chromatography Coupled to Inductively Coupled Plasma - Mass Spectrometric Detection with Collision Cell. Anne P. Vonderheide, University of Cincinnati, Department of Chemistry, Mail Location 0172, Cincinnati OH 45223-0172, pawleca@email.uc.edu; Juris Meija, Katherine Tepperman, Alvaro Puga, Allan R. Pinhas, J. Christopher States, and Joseph A. Caruso
FP24 Analysis of Hexavalent Chromium From Alkaline Digestion EPA 3060A Using Octopole Reaction System Agilent 7500cs. Marshall Pattee, North Creek Analytical, 9405 SW Nimbus Avenue, Beaverton OR 97008-7132, mpattee@ncalabs.com; Mutahsan Farooqui
FP25 Analysis of Wastewater and Mine Tailing Samples Using Octopole Reaction System Agilent 7500cs for Sub Parts Per Billion Reporting Levels. Marshall Pattee, North Creek Analytical, 9405 SW Nimbus Avenue, Beaverton OR 97008-7132, mpattee@ncalabs.com
FP26 Effects of Temperature and Ionic Strength on the Formation of Yttrium and REE Fluoride Complexes. Yanxin Luo, University of Miami, Rosenstiel School of Marine and Atmospheric Sci, 4600 Rickenbacker Cswy, Miami FL 33149-1098, yxluo@rsmas.miami.edu; Frank J. Millero
FP27 MC-ICPMS Studies of Anthropogenic Hf in the Environment. Michael E. Ketterer, Northern Arizona University, Department of Chemistry, Box 5698, Flagstaff AZ 86011-5698, michael.ketterer@nau.edu; August Keksis and William C. Wetzel
FP28 ICP-MS Determination of Environmental Beryllium Collected on Air Filters and Aerogel. Scott C. Szechenyi, Lawrence Livermore National Laboratory, L-232, PO Box 808, Livermore CA 94551-0808, szechenyi1@llnl.gov; Mark Sutton, Richard K. Bibby, Everett B. Guthrie, and Bradley K. Esser
FP29 High Accuracy Multi-Collector Isotope Dilution Mass Spectrometry of PGE's in Catalysts. Lorna Simpson, LGC Ltd., Queen's Road, Teddington, Middlesex TW11 0LY, United Kingdom, lorna.simpson@lgc.co.uk; Ruth Hearn and Peter Evans
FP30 Measurement of Sulphur and Chloride by Collision Cell, Multi-Collector ICP-MS. Zenon Palacz, GV Instruments, Crews Road, Wythenshawe, Manchester M23 9BE, United Kingdom, zenon.palacz@gvinstruments.co.uk; Simon Main, Patrick Turner, and Steve Shuttleworth
FP31 Platform ICP for the Routine Analysis of Water Samples: Meeting the Industry Regulations. Fadi Abou-Shakra, GV Instruments, Crews Road, Wythenshawe, Manchester M23 9BE, United Kingdom, fadi.aboushakra@gvinstruments.co.uk; Lucy Bunce and Steve Shuttleworth
FP32 Determination of 129I in Soil Samples Using On-line Gaseous Introduction in ICP-MS with Collision Cell. Andrei V. Izmer, Research Centre Jülich GmbH, Central Department for Chemical Analysis, Postfach 1913, D-52425 Jülich, Germany, a.izmer@fz-juelich.de; J. Sabine Becker
FP33 A Study of Polyatomic Interferences in ICP-MS. Jill W. Ferguson, Ames Laboratory USDOE, B5 Spedding Hall, Iowa State University, Ames IA 50011, jwfergus@iastate.edu; Elizabeth McKinney, Mark S. Gordon, and R.S. Houk
FP34 Molecular and Inductively Coupled Plasma Mass Spectrometric Study of Sugar Polyatomic Ions. Vivien F. Taylor, Trent University, Watershed Ecosystems, Peterborough ON K9J 7B8, Canada, vitaylor@trentu.ca; Henry P. Longerich, Ray E. March
FP35 Study on Interference of Polyatomic Ions in Isotope Ratio Measurement of Actinides by ICP-MS. Masaaki Magara, Japan Atomic Energy Research Institute, Department of Environmental Sciences, Tokai-mura, Naka-gum, Ibaraki 319-1195, Japan, magara@clear.tokai.jaeri.go.jp; Seiji Ichimura, Masato Takahasi, Setsumi Kurosawa, Yoko Saito, Fumitaka Esaka, Kenichiro Yasuda, Stoshi Skurai, Jy Chi, Kazuo Watanabe, and Shigekazu Usuda
FP36 Use of an Improved Lock Mass Technique for the Routine Analysis of Ultra-Low Concentrations by Sector Field ICP-MS. Lothar Rottmann, Thermo Electron (Bremen) GmbH, Barkhausenstr. 2, D-28197 Bremen, Germany, lothar.rottmann@thermo.com; Jürgen Lerche
FP37 Trace and Ultra-trace Metals Determination in Crude Oil and Fractions by inductively coupled plasma mass spectrometry (Q-ICP/MS and HR/ICP/MS). Sébastien Dreyfus, Université de Pau, CNRS UMR 5034, Hélioparc, 2 Avenue du Président Angot, F-64000 Pau, France, olivier.donard@univ-pau.fr; C. Pecheyran, H. Garraud, C.P. Lienemann, A. Prinzhofer, C. Magnier, and O.F.X. Donard
FP38 Accurate Determination of Sulfur and Trace Elements in Gasoline Using Isotope Dilution ICP-MS with Direct Sample Injection. Sergei F. Boulyga, Johannes Gutenberg-University Mainz, Institute for Inorganic Chemistry and Analytical, Duesbergweg 10-14, D-55099 Mainz, Germany, boulyga@uni-mainz.de; Jens Heilmann, and Klaus G. Heumann
FP39 Determination of 90Sr at Ultratrace Levels in Urine by ICP-MS. Anne P. Vonderheide, Research Centre Jülich GmbH, Central Department for Chemical Analysis, Postfach 1913, D-52425 Jülich, Germany, pawleca@email.uc.edu; Myroslav Zoriy, A. Izmer, Carola Pickhardt, Joseph A. Caruso, P. Ostapczuk, and J.S. Becker
FP40 Determination of 90Sr and 137Cs by ICP-MS. Vivien Taylor, Trent University, Watershed Ecosystems, Peterborough ON K9J 7B8, Canada, vitaylor@trentu.ca; R.D. Evans, and R.J. Cornett
FP41 Characterization of a Sealed 137Cs Radiation Source by Inductively Coupled Plasma Mass Spectrometry (ICP-MS). Daniel Cummings, Argonne National Laboratory - West, P.O. Box 2528, Idaho Falls ID 83404, dan.cummings@anlw.anl.gov; Mary Adamic, Kevin Carney, and Jeffrey Giglio
FP42 Determination of Stable and Radioactive Cs by IC-ICP-MS. Vladimir N. Epov, Trent University, Environmental and Resource Studies, 1600 West Bank Drive, Peterborough ON K9J 7B8, Canada, vepov@trentu.ca; Dominic Larivičre, R. Douglas Evans, and R. Jack Cornett
FP43 Analysis of Irradiated Samples by Atomic Spectrometric Methods. Pamela Crane, Argonne National Laboratory - West, P.O. Box 2528, Idaho Falls ID 83404, pamela.crane@anlw.anl.gov; Daniel Cummings, Kevin Carney, and Jeffrey Giglio
FP44 Determination of Spent Uranium Fuel and Calculation of its Burn-up in Nuclear Fallouts After the Accident at Chernobyl NPP. Sergei F. Boulyga, Johannes Gutenberg-University Mainz, Institute for Inorganic Chemistry and Analytical, Duesbergweg 10-14, D-55099 Mainz, Germany, boulyga@uni-mainz.de; Vladislav P. Mironov, Janna L. Matusevich, Vladimir P. Kudrjashov, Piotr I. Ananich, Vladimir V. Zhurvkov, and J. Sabine Becker
FP45 Overview of the Analytical Processes Used to Simplify Atom Percent Fission Analysis in Uranium and Plutonium Fuels By ASTM E321-96. Joseph M. Giaquinto, Oak Ridge National Laboratory, 1 Bethel Valley Rd, Bldg 2026, MS 6043, Oak Ridge TN 37831-6043, giaquintojm@ornl.gov; John M. Keller, Roosevelt Merriweather
FP46 Reducing Uranium Hydride Interference for the Measurement of Plutonium in Environmental and Biological Sample by ICP-MS. Chunsheng Li, Health Canada, Radiation Protection Bureau, 775 Brookfield Rd, Ottawa ON K1A 1C1, Canada, li_chunsheng@hc-sc.gc.ca; Vladimir Vais, Sonia Johnson, Dorothy Meyerhof, and Jack Cornett
FP47 Environmental Monitoring of Long-Lived Radionuclides at Ultratrace Level in Water Samples from Sea of Galilee by ICP-SFMS and MC-ICP-MS. Myroslav V. Zoriy, Research Centre Jülich GmbH, Central Department for Chemical Analysis, Postfach 1913, D-52425 Jülich, Germany, m.zoriy@fz-juelich.de; P. Ostapczuk, Ludwik Halicz, I.T. Platzner, Carola Pickhardt, C. Mueller, and J.S. Becker
FP48 239+240Pu and Stable Lead Chronologies of Lake Erie Sediments Determined by Sector ICPMS. Michael E. Ketterer, Northern Arizona University, Department of Chemistry, Box 5698, Flagstaff AZ 86011-5698, michael.ketterer@nau.edu; Gary D. MacLellan, Gerald Matisoff, and Christopher J. Wilson
FP49 Inventories and Depth Distributions of 239+240Pu in Background and Contaminated Soils Determined by Sector ICPMS. Michael E. Ketterer, Northern Arizona University, Department of Chemistry, Box 5698, Flagstaff AZ 86011-5698, michael.ketterer@nau.edu; Gary D. MacLellan, Wendy J. Hartsock, and Craig Asplund
FP50 Separation of Actinides at Ultra-Trace Level From Urine Matrix by Ion Chromatography-ICP-Q-MS. Wenwan Zhong, Los Alamos National Laboratory, P.O. Box 1663, C-ACS, MS K484, Los Alamos NM 87545, weihang@lanl.gov; Wei Hang, Luwang Zhu, and Cynthia Mahan
FP51 Uranium Isotopic Ratio Measurement in Human Urine by HR-ICP-MS with an APEX Sample Introduction System. Bill Ting, Centers for Disease Control & Prevention, 4770 Buford Hwy NE, Mail Stop F-18, Atlanta GA 30341-3724, rlj0@cdc.gov; Robert L. Jones, and Kathleen L. Caldwell
FP52 High Precision U Isotope Ratio Measurement by MC-ICP-MS. Qianli Xie, Trent University, Water Quality Centre, ERS Program, Peterborough ON K9J 7B8, Canada, qianlixie@trentu.ca; Peter Dillon, and Doug Evans
FP53 Pb-210 by ICP-MS at the Environmental Level: An Analytical Challenge. Dominic Larivičre, Trent University, Department of Chemistry, 1600 West Bank Drive, Peterborough ON K9J 7B8, Canada, dlarivie@trentu.ca; R. Douglas Evans, and R. Jack Cornett
FP54 Mercury, Lead, and Cadmium Analysis in Whole Blood by ICP-MS: Comparison of ICP-MS and GF-AAS for Lead and Cadmium Analysis, ICP-MS and CV-AAS fo Hg Analysis. Olga Piraner, Centers for Disease Control & Prevention, 4770 Buford Hwy NE, Mail Stop F-18, Atlanta GA 30341-3724, jhj8@cdc.gov; Kathleen L. Caldwell, Janie Mullinix, Ron Albalak, and Robert L. Jones
FP55 Use of ICP-MS for Evaluation of Population Exposures to Trace and Toxic Metals. Robert L. Jones, Centers for Disease Control & Prevention, 4770 Buford Hwy NE, Mail Stop F-18, Atlanta GA 30341-3724, rlj0@cdc.gov; Kathleen L. Caldwell, Carol Rubin, and Ken Orloff
FP56 Measurement of Calcium Isotope Ratios Using a Collision Cell Interfaced Multi-Collector ICPMS. Zenon Palacz, GV Instruments, Crews Road, Wythenshawe, Manchester M23 9BE, United Kingdom, zenon.palacz@gvinstruments.co.uk; Simon Main, and Patrick Turner
FP57 Novel Dynamic In Vitro Method to Assess the Bio-Accessibility of Elements from Food Using Flow Injection and Inductively Coupled Plasma Mass Spectrometry. Diane Beauchemin, Queen's University, Department of Chemistry, Kingston ON K7L 3N6, Canada, beauchmn@chem.queensu.ca; Mingyan Chu
FP58 Synthesis and Application of Isotopically Labelled Selenomethionine for Isotope Dilution Analysis Using HPLC-ICP-MS. J. Igancio García Alonso, University of Oviedo, Department of Physical and Analytical Chemistry, Julian Caveria 8, E-33006 Oviedo, Spain, ngalonso@correo,uniovi.es; Laura Hinojosa Reyes, J.M. Marchante Gayón, and Alfredo Sanz-Medel
FP59 Kinetic and Equilibrium Fe Isotope Fractionation During Redox Cycling of Fe in Seasonally Anoxic Lake Water. Dmitry Malinovsky, Luleĺ University of Technology, Division of Applied Geology, SE-97187 Luleĺ, Sweden, dima@sb.luth.se; Jerry Forsberg, Larisa Pekka, Henrik Andren, Anna Stenberg, Douglas C. Baxter, Björn Öhlander, Willis Forsling, Johan Ingri, Ilia Rodushkin, and Crister Pontér
5:00 – 6:30 Social Mixer
Panel Discussion
5:30 PD04 Plasma Source Mass Spectrometry for Real-Life Applications. Luc Moens and Frank Vanhaecke, Ghent University, Laboratory of Analytical Chemistry, Proeftuinstraat 86, B-9000 Ghent, Belgium, luc.moens@ugent.be; Bob Botto, Mike Ketterer, Joe Brenner, and Thomas Walczyk
Saturday, January 10, 2004
11. Plasma Source Mass Spectrometry: Applications and Stable Isotope Analysis
Conrad Grégoire, Chair
08:00 PL06 Isotope Ratio Measurements with ICP-MS: High End and Low End Instruments and Applications. Luc Moens and Frank Vanhaecke, University of Ghent, Laboratory of Analytical Chemistry, Proeftuinstraat 86, B-9000 Gent, Belgium, luc.moens@ugent.be
09:00 IL18 Isotope Dilution LA - ICP - MS: A New Calibration Method for Trace Element Determination in Powdered Solid Samples? Klaus G. Heumann, Johannes Gutenberg - Universität Mainz, Institute of Inorganic Chemistry, Duesbergweg 10-14, D-55099 Mainz, Germany, heumann@mail.uni-mainz.de; Markus Tibi, and Sergei Boulyga
09:30 IL19 Multilabelled Speciated Isotope Dilution ICP-MS: The Way to Reliable Quantitative Chemical Speciation. José Ignacio Garcia Alonso, University of Oviedo, Department of Chemistry, Julian Claveria 8, E-33006 Oviedo, ngalonso@correo.uniovi.es
10:00 Break
10:20 S01 Variation in Isotope Ratios During Transient Signals Using Chromatography: Instrumental or Chromatographic Effect? R. Douglas Evans, Trent University, Environmental Science Centre, 1600 West Bank Dr., Peterborough ON K9J 7B8, Canada, devans@trentu.ca; Qianli Xie, and Peter Dilon
10:40 S02A Flow Injection System with On-line Dialysis for Trace Element Determination in Serum Samples by Isotope Dilution Inductively Coupled Plasma Mass Spectrometry. Maria Fernanda Giné Rosias, Centro de Energia Nuclear na Agricultura, Universidade de Sao Paulo, Av. Centerárlo 303, CEP 13416-970, Piracicaba SP, Brazil, mfgine@cena.usp.br; Ana Cláudia S. Bellato, and Amauri A. Menegário
11:00 S03 Quantitative Determination of Uranium and Uranium 235/238 Ratios in Human Urine Using Isotopic Dilution - Inductively Coupled Plasma -Mass Spectrometry (ID-ICP-MS). David N. Kurk, DoD - US Army CHPPM, MCHB-TS-LRD, 5158 Blackhawk Road, APG-EA, MD 21010-5403, david.kurk@apg.amedd.army.mil; Ronald J. Swatski
11:20 S04 Transport of Trace Metals in the Kalix River; FiFFF-HR-ICP-MS Analysis of Temporal Variations in the Composition and Size Distributions of Natural Water Colloids and Associated Elements. Karen Andersson, Göteborg University, Department of Chemistry, Analytical and Marine Chemistry, SE-412 96 Göteborg, Sweden, karen@amc.gu.se; Björn Stolpe, Tobias Larsson, and David Turner
11:40 S05 Determination of Radionuclides in Drinking Water by Sector Field ICP-MS. Meike Hamester, Thermo Electron, Barkhausenstr. 2, D-28197 Bremen, Germany, meike.hamester@thermo.de; Julian D. Wills
12:00 Lunch Break
Saturday, January 10, 2004
12. Plasma Source Mass Spectrometry: Applications and High Resolution Analysis
J. Sabine Becker, Chair
1:00 IL20 New Concepts for Using MC-ICP-MS in Biomedical Research. Thomas Walczyk, ETH Zürich Swiss Federal Institute of Technology, Laboratory of Human Nutrition, Seestrasse 72, CH-8803 Rüschlikon, Switzerland, thomas.walczyk@ilw.agrl.ethz.ch
1:30 IL21 Quo Vadis: Applications of MC-ICPMS in Environmental Geochemistry. Michael E. Ketterer, Northern Arizona University, Department of Chemistry, Box 5698, Flagstaff AZ 86011-5698, michael.ketterer@nau.edu
2:00 S06 Precise Measurement of Li Isotopes by MC-ICP-MS and Comparison with TIMS Analyses. Romain Millot, BRGM French Geological Survey, Service Analyse et Caractérisation Minérale, 3, aveue Claude Guillemin BP 6009, F-45060 Orléans Cedex 2, France, r.millot@brgm.fr; Catherine Guerrot, and Thomas D. Bullen
2:20 S07 The Determination of Burn-Up Using a 148Nd Method. A Comparative Study of Different Mass Spectrometric Techniques. Zlatko Kopajtic, Paul Scherrer Institut PSI, Department of Nuclear Energy and Safety, Laboratory of Materials Behavior, CH-5232 Villigen PSI, Switzerland, zlatko.kopajtic@psi.ch; Ines Günther-Leopold, and Beat Wernli
2:40 S08 A Comparison of the Accuracy and Uncertainty Achieved by High Resolution Magnetic Sector ICP-MS, ICP-OES and Collision Cell ICP-MS for the High Accuracy Determination of Ca in Serum. Lorna Simpson, LGC Ltd., Queen's Road, Teddington Middlesex TW11 0LY, United Kingdom, lorna.simpson@lgc.co.uk; Ruth Hearn and Sheila Merson
3:00 Break
3:20 S09 ICP-MS Analysis of Calcium Isotopes from Human Serum: An Acid Equilibration Method Requiring Low Sample Volume. Zhensheng Chen, Baylor College of Medicine, USDA/ARS Children's Nutrition Research Center, 1100 Bates Street, Houston TX 77030, zchen1@bcm.tmc.edu; Ian J. Griffin, Yana L. Kriseman, Lily K. Liang, Steven A. Abrams
3:40 S10 Natural Iron Isotopic Variation in Individuals with HFE Mutations. Jurian Hoogewerff, Institute of Food Research, Norwich Research Park, Colney, Norwich NR4 7UA, United Kingdom, jurian.hoogewerff@bbsrc.ac.uk; Mark Roe, Jack Dainty, Christian Wolf, Brigit Teucher, and Sue Fairweather-Tait
4:00 S11 Iron Isotopic Fractionation During the Dissolutive Reduction of Synthetic Iron Oxides by Micro-Organisms. Mikael Motelica-Heino, BRGM French Geological Survey, Service Analyse et Caractérisation Minérale, 3, avenue Claude Guillemin BP 600, F-45060 Orléans Cedex 2, France, m.millot@brgm.fr; L. Hughet, G. Diot, and F. Garrido
4:20 S12 Determination of Traffic-Related Pt and Rh Concentrations in Airborne Particulate Matter from Buenos Aires. Sergio Caroli, Istituto Superiore di Sanitŕ, Viale Regina Elena 299, I-00161 Rome, Italy, caroli@iss.it; B. Bocca, S. Caimi, P. Smichowski, D. Gómez
4:40 S13 Development and Validation of a Sub-ppt ICP-MS Method for Pt Determination in Rat Plasma and Ultrafiltrate by the Hot Plasma Technique. Claudio Mucchino, Universita di Parma, Dipartimento di Chimica Generale ed Inorganica, Parco Area delle Scienze 17/a, I-43100 Parma, Italy, claudiom@unipr.it; Monica Maffini, Alessandro Mangia, and Patrice Larger
5:00 IL22 Unexplored Directions of HR ICP-MS. J. Sabine Becker, Research Centre Jülich, Central Department for Chemical Analysis, D-52425 Jülich, Germany, s.becker@fz-juelich.de
Panel Discussion
5:30 PD05 New Plasma Source Mass Spectrometers. Norbert Jakubowski, Institute for Spectrochemistry, and Applied Spectroscopy, P.O. Box 10 13 52, D-44013 Dortmund, Germany, jakubowski@isas-dortmund.de; Ralph Sturgeon, Joseph A. Caruso, and John Olesik
6:30 Conference Closing Ceremony
For program, registration, hotel, and transportation details, contact Ramon Barnes, ICP Information Newsletter, Inc., P.O. Box 666, Hadley, MA 01003-0666. Phone: 413-256-8942, fax 413-256-3746, e-mail winterconf@chem.umass.edu, http://www.chem.umass.edu/WinterConf2004.
2004
Winter Conference on Plasma Spectrochemistry
%ICP
Information Newsletter, Inc., P.O. Box 666, Hadley, MA 01035-0666
Dr.
Ramon Barnes, Conference Chairman, Telephone (413) 256-8942, Fax (413) 256-3746
email wc2004@chemistry.umass.edu, http://www-unix.oit.umass.edu/~wc2004
Last Updated: December 3, 2003